Development of a selective homonuclear dipolar recoupling method in magic-angle spinning solid-state NMR and its application to the structural analysis of a molecule マジック角度回転固体NMRにおける同種核間双極子相互作用の選択的復活法の開発と分子の構造解析への応用
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著者
書誌事項
- タイトル
-
Development of a selective homonuclear dipolar recoupling method in magic-angle spinning solid-state NMR and its application to the structural analysis of a molecule
- タイトル別名
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マジック角度回転固体NMRにおける同種核間双極子相互作用の選択的復活法の開発と分子の構造解析への応用
- 著者名
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野村, 薫
- 著者別名
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ノムラ, カオル
- 学位授与大学
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京都大学
- 取得学位
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博士 (理学)
- 学位授与番号
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甲第7687号
- 学位授与年月日
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1999-03-23
注記・抄録
博士論文
目次
- 論文目録 / (0001.jp2)
- Contents / p1 (0005.jp2)
- Abstruct / p4 (0008.jp2)
- 1 Introduction / p6 (0010.jp2)
- 2 NMR Spectra of Homonuclear Spin-1/2 Pairs Dipolar-Recoupled by Radio-Frequency Field Irradiation under Magic-Angle Spinning / p11 (0015.jp2)
- 2.1 Introduction / p11 (0015.jp2)
- 2.2 Theory / p14 (0018.jp2)
- 2.3 Results and discussion / p37 (0041.jp2)
- 2.4 Conclusion / p45 (0049.jp2)
- Appendix1 Line splitting of the powder line shapes / p48 (0052.jp2)
- 3 Selective Homonuclear Polarization Transfer in the Tilted Rotating Frame under Magic Angle Spinning in Solids / p58 (0072.jp2)
- 3.1 Introduction / p58 (0072.jp2)
- 3.2 Theory / p61 (0075.jp2)
- 3.3 Experimental results and discussion / p69 (0083.jp2)
- 3.4 Conclusion / p79 (0093.jp2)
- 4 Determination of the Complete Structure of a Uniformly Labeled Molecule by Rotational Resonance Solid-State NMR in the Tilted Rotating Frame / p84 (0108.jp2)
- 4.1 Introduction / p84 (0108.jp2)
- 4.2 Method of Structure Determination / p86 (0110.jp2)
- 4.3 Experimental results and discussion / p89 (0113.jp2)
- 4.4 Conclusion / p103 (0127.jp2)
- References / p110 (0147.jp2)
- Acknowledgements / p118 (0155.jp2)
- Frequency Response Method for Study of Kinetic Details of a Heterogeneous Catalytic Reaction of Gases.2.A Methanol Conversion to Olefins / p3319 (0187.jp2)
