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Studies on electrospray ionization mass spectrometry of microcystins, cyclic heptapeptide hepatoxins, produced by cyanobacteria

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著者

    • 袁, 謀村 エン, ボウソン

書誌事項

タイトル

Studies on electrospray ionization mass spectrometry of microcystins, cyclic heptapeptide hepatoxins, produced by cyanobacteria

著者名

袁, 謀村

著者別名

エン, ボウソン

学位授与大学

東京水産大学

取得学位

博士(水産学)

学位授与番号

甲第173号

学位授与年月日

1999-03-25

注記・抄録

博士論文

目次

  1. Contents / p1 (0003.jp2)
  2. Chapter1:Introduction(Part A)Toxins from cyanobacteria(blue-green algae) / p1 (0008.jp2)
  3. 1.1 Cyanobacteria and blue-green algae / p1 (0008.jp2)
  4. 1.2 Toxins of cyanobacteria / p4 (0011.jp2)
  5. 1.3 Hepatotoxins produced by toxic cyanobacteria / p7 (0014.jp2)
  6. 1.4 Isolation and purification of toxic peptides from freshwater cyanobacteria / p14 (0021.jp2)
  7. 1.5 General method for structure assignment of toxic cyclic peptides / p17 (0024.jp2)
  8. 1.6 Current situation and trends of studies on cyanobacteria toxins / p19 (0026.jp2)
  9. Chapter2:Introduction(Part B)Mass spectrometry and structure assignment of peptides / p21 (0028.jp2)
  10. 2.1 Methods of ion production-soft ionization / p21 (0028.jp2)
  11. 2.2 Study methods of ion fragmentations:Collision-induced dissociation(CID) / p27 (0034.jp2)
  12. 2.3 Determining the molecular weight of proteins and peptides by ESIMS / p28 (0035.jp2)
  13. 2.4 Mass spectrometric determination of the amino acid sequence of proteins and peptides / p33 (0040.jp2)
  14. 2.5 Protonation site of proteins and peptides in solution and fragmentation of ions in gas phase / p35 (0042.jp2)
  15. 2.6 FABMS and FABMS/CID/MS of microcystins / p38 (0045.jp2)
  16. Chapter3:Electrospray ionization mass spectrometric analysis of microcystins,cyclic heptapeptide hepatotoxins:Modulation of charge states and〔M+H〕⁺to〔M+Na〕⁺ratio / p39 (0046.jp2)
  17. 3.1 Introduction / p40 (0047.jp2)
  18. 3.2 Experimental / p41 (0048.jp2)
  19. 3.3 Results and Discussion / p44 (0051.jp2)
  20. 3.4 Conclusions / p69 (0076.jp2)
  21. Chapter4:Low-Energy Collisionally Activated Decomposition and Structural Characterization of Cyclic Heptapeptide Microcystins by Electrospray Ionization Mass Spectrometry / p71 (0078.jp2)
  22. 4.1 Introduction / p72 (0079.jp2)
  23. 4.2 Experimental / p73 (0080.jp2)
  24. 4.3 Results and Discussion / p74 (0081.jp2)
  25. 4.4 Conclusions / p97 (0104.jp2)
  26. Chapter5:Effect of Amino Acid Side-chain on Fragmentation of Cyclic Peptide Ions:Differences of ESIMS/CID/mass Spectra of Toxic Heptapeptide Microcystins Containing ADMAdda instead of Adda / p100 (0107.jp2)
  27. 5.1 Introduction / p101 (0108.jp2)
  28. 5.2 Experimental / p102 (0109.jp2)
  29. 5.3 Results and Discussion / p104 (0111.jp2)
  30. 5.4 Conclusions / p119 (0126.jp2)
  31. Chapter6:Application / p123 (0130.jp2)
  32. 6.1 Characterization of known microcystins / p124 (0131.jp2)
  33. 6.2 Structure assignment of seven new microcystins possessing two L-glutamic acid units,isolated from Anabaene sp.strain 186 / p128 (0135.jp2)
  34. Chapter7:Discussion / p136 (0143.jp2)
  35. 7.1 Effective factors of cyclic and linear peptides in electrospray ionization mass spectrometry / p136 (0143.jp2)
  36. 7.2 Enlightenment from the structure assignment of two types of cyclic compounds by mass spectrometry / p137 (0144.jp2)
  37. 7.3 Mechanisms of fragmentation of microcystins in ESIMS/CID/MS / p140 (0147.jp2)
  38. 7.4 Negative ion ESIMS analysis of microcystins / p142 (0149.jp2)
  39. Chapter8:Summary / p149 (0156.jp2)
  40. Chapter9:References / p154 (0161.jp2)
  41. Acknowledgments / (0172.jp2)
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各種コード

  • NII論文ID(NAID)
    500000172601
  • NII著者ID(NRID)
    • 8000000172877
  • DOI(NDL)
  • NDL書誌ID
    • 000000336915
  • データ提供元
    • NDL-OPAC
    • NDLデジタルコレクション
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