Synthesis of Fe-Cr Alloys by Mechanical Alloying and its Consolidation.

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  • 金属間化合物の粉末冶金と諸物性 メカニカルアロイング法によるFe‐Cr合金の合成とその固化成形
  • メカニカル アロイングホウ ニヨル Fe-Cr ゴウキン ノ ゴウセイ ト ソ

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Abstract

Fe32Cr68, Fe42Cr58, Fe52Cr48, Fe62Cr38 and Fe72Cr28 were synthesized by mechanical alloying (MA) of Fe powder and Cr powder using a planetary ball milling for 180ks in 1.33kPa argon gas atmosphere. In particular, the influence of milling time on structural phase of Fe52Cr48 has been studied. Because according to the phase diagram, a phase is expected to form on the composition of Fe52Cr48. As the Cr content of MA powder increased, the time for homogenization by MA became longer.<BR>These MA powders were compacted by Spark Plasma Sintering (SPS) process. Mechanical alloyed Fe52Cr48 was rapidly shrunk at above 800K and completely condensed above 1073K. Fe52Cr48 which compacted by SPS at 1073K had no pore and its density was 7.46g/cm3.<BR>Fe-Cr alloy prepared by this process contained no σ-phase.

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