高周波誘導型高密度プラズマを用いた純鉄の窒化

書誌事項

タイトル別名
  • Nitriding of Pure Iron in High-density Plasma Using Inductively Coupled Radio Frequency Discharge.
  • コウシュウハ ユウドウガタ コウミツド プラズマ オ モチイタ ジュンテツ ノ チッカ

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抄録

High-density RF induction plasma having a density of 1013cm-3 was generated using 13.56MHz 350W RF power Anticipating the effect of high-density ions, we applied the high-density nitrogen plasma to surface nitriding of iron A nitrided layer consisting of Fe3N and Fe4N was obtained at 550°C without applying a bias voltage When -200V of bias voltage was applied to the iron substrate, the main product at the surface was Fe3N having a higher nitrogen content than Fe3N obtained without bias voltage This bias voltage enabled us to nitride the iron surface even at 350°C The Vickers hardness of the surface obtained by conventional low-density plasma at 550°C was 360Hv Using high-density plasma, we obtained 980Hv Vickers hardness increased to 1390Hv when we applied a bias voltage of -100V The maximum hardness, 1410Hv, was obtained at 550°C by applying -200V The Vickers hardness of the surface prepared at 350°C with -200V bias voltage was 970Hv, comparable to that prepared at 550°C with no bias voltage The thickness of the nitriding layer obtained at 550°C with a bias voltage of -200V was 1.9μm, thinner than that obtained by conventional plasma under the same nitriding conditions We concluded that a large amount of nitrogen ion species in the high-density plasma significantly affects iron nitriding, especially surface hardness

収録刊行物

  • 表面技術

    表面技術 50 (2), 195-199, 1999

    一般社団法人 表面技術協会

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