Preparation of Micron-Size Monodisperse Silica Particles by Seed Growth Method.

• Kimata Mitsumasa

  Department of Materials Science and Engineering, Yamagata University

• Koizumi Mitsuhiro

  Department of Materials Science and Engineering, Yamagata University

• Hasegawa Masahiro

  Department of Materials Science and Engineering, Yamagata University

Bibliographic Information

Other Title

• シード粒子成長法によるミクロンサイズ単分散シリカ微粒子の調製
• シード リュウシ セイチョウホウ ニヨル ミクロン サイズ タン ブンサン シ

Abstract

Hydrolysis and condensation of tetraethyl orthosilicate (TEOS) with silica seed particles were carried out by a semi-batch operation for an efficient preparation of monodisperse silica particles with micron order size. In the reaction initiated by the continuous addition of TEOS, the nucleation of silica particles continued, regardless of the addition rate of TEOS. Monodisperse silica paticles of micron order size were efficiently obtained by the following semi-batch operation. The continuous addition of TEOS and water the reaction system after the transient batch process in which no nucleation takes place. It was also found that the diameter of silica particles given by the seed growth method of the semi-batch operation could be estimated accurately.

Journal

• KAGAKU KOGAKU RONBUNSHU

  KAGAKU KOGAKU RONBUNSHU 22 (6), 1366-1372, 1996

  The Society of Chemical Engineers, Japan

Keywords

• Monodisperse Silica Particle
• Seed Growth Method
• Hydrolysis
• Metal Alkoxide
• Tetraethoxysilan

Details

• CRID: 1390001204508538496
• NII Article ID: 10002669902
• NII Book ID: AN00037234
• DOI: 10.1252/kakoronbunshu.22.1366
• COI: 1:CAS:528:DyaK28XntFWkt7k%3D
• ISSN: 13499203
• ISSN: 0386216X
• ISSN: http://id.crossref.org/issn/0386216X
• NDL BIB ID: 4078154
• Web Site: https://ndlsearch.ndl.go.jp/books/R000000004-I4078154
• Web Site: http://www.jstage.jst.go.jp/article/kakoronbunshu1975/22/6/22_6_1366/_pdf
• Text Lang: ja
• Data Source:
  • JaLC
  • NDL
  • Crossref
  • CiNii Articles
• Abstract License Flag: Disallowed