A Route to Functionalized (η3-Allyl)dicarbonylnitrosyliron Complexes: Regio- and Stereoselective Acylmetallation of Allenes

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  • Keiji Itoh
    Department of Industrial Chemistry, Osaka Prefectural College of Technology
  • Saburo Nakanishi
    Department of Applied Chemistry, Graduate School of Engineering, Osaka Prefecture University
  • Toshikazu Takata
    Department of Applied Chemistry, Graduate School of Engineering, Osaka Prefecture University

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<jats:title>Abstract</jats:title> <jats:p>Allenes regio- and stereoselectively react with alkyl halides in the presence of tetrabutylammonium tricarbonylnitrosyl ferrate to give anti-(η3-2-acylallyl)dicarbonylnitrosyliron complexes in good yields. The reaction provides a convenient method for preparation of di- and trisubstituted η3-allyl iron complexes with acyl groups at the central carbon of the allylic ligands.</jats:p>

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  • Chemistry Letters

    Chemistry Letters 29 (6), 672-673, 2000-06-01

    Oxford University Press (OUP)

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