粉末製造技術とその評価  水熱法によるナノサイズ酸化物微粒子の合成

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タイトル別名
  • Hydrothermal Synthesis of Nano Sized Oxided Particles
  • スイネツホウ ニ ヨル ナノサイズ サンカブツ ビリュウシ ノ ゴウセイ

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抄録

We synthesized nano sized cerium and zirconium oxide particles by the hydrothermal treatment of precipitates formed from the chlorides of each metal ion. Especially the cerium oxide particles had plate-like shapes with the particle size in the range of 2-20 run. Even in the particle size of 2nm, most of the cerium oxide particles observed by a high resolution transmission electron microscope showed clear lattice images based on (111) and (200) planes indicating the plate-like single crystals. In the zirconium oxide particles, it was confirmed that the single phases of monoclinic and tetragonal crystals were obtained by the hydrothermal treatment lower than 200°C maintaining the particle size of about 10nm.

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