Growth of Pure β-Si_3N_4 Nanorods from the Synergic Nitrogen Sources

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著者

    • XU Fen
    • Structure Research Laboratory and Department of Chemistry, University of Science and Technology of China
    • ZHANG Xu
    • Structure Research Laboratory and Department of Chemistry, University of Science and Technology of China
    • XI Wang
    • Structure Research Laboratory and Department of Chemistry, University of Science and Technology of China
    • HONG Jie
    • Structure Research Laboratory and Department of Chemistry, University of Science and Technology of China
    • XIE Yi
    • Structure Research Laboratory and Department of Chemistry, University of Science and Technology of China

抄録

Pure β-Si<SUB>3</SUB>N<SUB>4</SUB> nanorods with of 30–60 nm and length of 180–300 nm were synthesized from a mild benzene-thermal route at 450 °C, starting from SiCl<SUB>4</SUB> and the synergic nitrogen sources of NaNH<SUB>2</SUB> and NH<SUB>4</SUB>Cl. The obtained sample was characterized by XRD, TEM and XPS. The one-dimensional growth mechanism is assumed to be a vapor-liquid-solid (VLS) process.

収録刊行物

  • Chemistry letters

    Chemistry letters 32(7), 600-601, 2003-07-05

    The Chemical Society of Japan

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各種コード

  • NII論文ID(NAID)
    10012817428
  • NII書誌ID(NCID)
    AA00603318
  • 本文言語コード
    ENG
  • 資料種別
    SHO
  • ISSN
    03667022
  • データ提供元
    CJP書誌  J-STAGE 
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