A Cationic Diruthenium Amidinate, [(η5-C5Me5)Ru(μ2-<i>i</i>-PrN=C(Me)N<i>i</i>-Pr)Ru(η5-C5Me5)]+, as an Efficient Catalyst for the Atom-Transfer Radical Reactions

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  • Yukihiro Motoyama
    Institute for Materials Chemistry and Engineering, Graduate School of Engineering Sciences, Kyushu University
  • Mitsuru Gondo
    Institute for Materials Chemistry and Engineering, Graduate School of Engineering Sciences, Kyushu University
  • Satoshi Masuda
    Institute for Materials Chemistry and Engineering, Graduate School of Engineering Sciences, Kyushu University
  • Yuya Iwashita
    Institute for Materials Chemistry and Engineering, Graduate School of Engineering Sciences, Kyushu University
  • Hideo Nagashima
    Institute for Materials Chemistry and Engineering, Graduate School of Engineering Sciences, Kyushu University

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<jats:title>Abstract</jats:title> <jats:p>A cationic diruthenium amidinate, [(η5-C5Me5)Ru(μ2-i-PrN=C(Me)Ni-Pr)Ru(η5-C5Me5)]+, is generated by treatment of (η5-C5Me5)Ru(μ2-i-PrN=C(Me)Ni-Pr)Ru(Cl)(η5-C5Me5) (3a) with NaPF6 or other metal salts of weakly coordinating anions, which is active towards catalytic atom transfer radical cyclization of N-allyl trichloroacetamides and related reactions.</jats:p>

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  • Chemistry Letters

    Chemistry Letters 33 (4), 442-443, 2004-03-20

    Oxford University Press (OUP)

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