Preparative Separation of Acanthoside-D from Acanthopanax senticosus

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抄録

<I>Acanthopanax senticosus</I> called Siberian Ginseng has not only a medical benefit for tonic, lumbago, neuralgia and palsy, but also an active operation on metabolism. In this work, the <I>A. senticosus</I> was purchased from Korea Siberian Ginseng Association. The ethanol extract from the powder of the trunk of <I>A. senticosus</I> was partitioned with water and hexane. The resulting solution was purified on a preparative column (3.9 × 300 mm, 15 <I>μ</I>m, Lichrospher 100RP-18). The mobile phase composition for isolating <I>acanthoside-D</I> from extract was water/acetonitrile/methanol, 80/14/6%(v/v). The flow rate of mobile phase was 1 m<I>l</I>/min and the UV wavelength was fixed at 210 nm. The fraction containing <I>acanthoside-D</I> was collected and concentrated about one hundred times by a rotary evaporator. From the chromatogram, the impurities were almost eliminated and only pure <I>acanthoside-D</I> was obtained. Finally on a preparative column (3.9 × 300 mm, 15 <I>μ</I>m, Lichrospher 100RP-18) with the same mobile phase composition, the allowable maximum injection volume increased to 500 <I>μ</I><I>l</I>.

収録刊行物

  • Journal of chemical engineering of Japan

    Journal of chemical engineering of Japan 37(2), 378-382, 2004-02-01

    公益社団法人 化学工学会

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各種コード

  • NII論文ID(NAID)
    10013339709
  • NII書誌ID(NCID)
    AA00709658
  • 本文言語コード
    ENG
  • 資料種別
    SHO
  • ISSN
    00219592
  • NDL 記事登録ID
    6863185
  • NDL 雑誌分類
    ZP1(科学技術--化学・化学工業)
  • NDL 請求記号
    Z53-R395
  • データ提供元
    CJP書誌  NDL  J-STAGE 
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