Synthesis of Novel Well-defined End-functional Macrophotoinitiator of Poly(ε-caprolactone) by Ring-opening Polymerization

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A new end-chain functional macrophotoinitiator of poly(ε-caprolactone) has been synthesized by controlled/living ring-opening polymerization (ROP) method. For this purpose, mono hydroxy functional a photoinitiator namely, 1-hydroxycyclohexyl phenyl ketone (HCPK), Irgacure 184, was used as the initiator for the stannous-2-ethylhexanoate (Sn(Oct)<SUB>2</SUB>) catalyzed living ring-opening polymerization of ε-caprolactone. The GPC and IR, H NMR, UV and fluorescence spectroscopic studies revealed that low-polydispersity poly(ε-caprolactone) with photoinitiator functionality at the end of the chain was obtained.

収録刊行物

  • Polymer journal

    Polymer journal 36(7), 542-548, 2004-07-15

    社団法人 高分子学会

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各種コード

  • NII論文ID(NAID)
    10013342518
  • NII書誌ID(NCID)
    AA00777013
  • 本文言語コード
    ENG
  • 資料種別
    ART
  • ISSN
    00323896
  • NDL 記事登録ID
    7009091
  • NDL 雑誌分類
    ZP16(科学技術--化学・化学工業--高分子化学・高分子化学工業)
  • NDL 請求記号
    Z53-R487
  • データ提供元
    CJP書誌  NDL  J-STAGE 
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