Determination of Bisphenol-A in Water by Semi-Micro Column High-Peformance Liquid Chromatography Using 2-Methoxy-4-(2-phthalimidinyl)-phenylsulfonyl Chloride as a Fluorescent Labeling Reagent
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- TSURUTA Yasuto
- Faculty of Pharmacy and Pharmaceutical Sciences, Fukuyama University
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- INOUE Hirofumi
- Faculty of Pharmacy and Pharmaceutical Sciences, Fukuyama University
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- FUKUNAGA Keiko
- Faculty of Pharmacy and Pharmaceutical Sciences, Fukuyama University
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- MUNEMURA Sayaka
- Faculty of Pharmacy and Pharmaceutical Sciences, Fukuyama University
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- OZAKI Misa
- Faculty of Pharmacy and Pharmaceutical Sciences, Fukuyama University
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- OHTA Masaya
- Department of Biotechnology, Faculty of Life Science and Biotechnology, Fukuyama University
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- MATSUURA Fumito
- Department of Biotechnology, Faculty of Life Science and Biotechnology, Fukuyama University
書誌事項
- タイトル別名
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- Determination of Bisphenol-A in Water by Semi-Micro Column High-Performance Liquid Chromatography Using 2-Methoxy-4-(2-phthalimidinyl)-phenylsulfonyl Chloride as a Fluorescent Labeling Reagent
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抄録
A highly sensitive method for the determination of bisphenol-A in water with semi-micro column high-performance liquid chromatography using 2-methoxy-4-(2-phthalimidinyl)phenylsulfonyl chloride as a fluorescent labeling reagent has been developed. The labeling reaction was carried out at 70°C for 20 min in borate buffer (pH 9.5). The derivative eluted at 11.6 min on a reversed-phase column with methanol-water (78:22, v/v) at a flow-rate of 0.2 ml/min. The fluorescence was monitored at 308 nm for excitation and 410 nm for emission. The detection limit (S/N = 3) was 10 fmol per injection. The labeling yield was about 95%.
収録刊行物
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- Analytical Sciences
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Analytical Sciences 21 (6), 697-699, 2005
社団法人 日本分析化学会
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詳細情報 詳細情報について
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- CRID
- 1390282679232472704
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- NII論文ID
- 10016141995
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- NII書誌ID
- AA10500785
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- COI
- 1:CAS:528:DC%2BD2MXlsFersLo%3D
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- ISSN
- 13482246
- 09106340
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- NDL書誌ID
- 7332775
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- PubMed
- 15984209
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- NDL
- Crossref
- PubMed
- CiNii Articles
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- 抄録ライセンスフラグ
- 使用不可