Electronically Tunable Compact Trialkylphosphines: SMAPs-bridged Bicyclic Phosphines

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  • Atsuko Ochida
    Division of Chemistry, Graduate School of Science, Hokkaido University, and PRESTO, JST
  • Shinichiro Ito
    Division of Chemistry, Graduate School of Science, Hokkaido University, and PRESTO, JST
  • Takahiro Miyahara
    Division of Chemistry, Graduate School of Science, Hokkaido University, and PRESTO, JST
  • Hajime Ito
    Division of Chemistry, Graduate School of Science, Hokkaido University, and PRESTO, JST
  • Masaya Sawamura
    Division of Chemistry, Graduate School of Science, Hokkaido University, and PRESTO, JST

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<jats:title>Abstract</jats:title> <jats:p>A series of silicon-constrained monodentate trialkylphosphines SMAPs bearing a Si substituent with diverse electronic natures were synthesized. DFT calculations and NMR measurements indicated that these compounds constitute a class of electronically tunable trialkylphosphines. The tunable range of donor power overlaps those of tri(tert-butyl)phosphine and monoalkyldiarylphosphines.</jats:p>

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  • Chemistry Letters

    Chemistry Letters 35 (3), 294-295, 2006-03-01

    Oxford University Press (OUP)

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