Graphical Synthesis of an Internally Heat-Integrated Distillation Column

  • Huang Kejin
    Research Institute for Innovation in Sustainable Chemistry, National Institute of Advanced Industrial Science and Technology (AIST)
  • Matsuda Keigo
    Research Institute for Innovation in Sustainable Chemistry, National Institute of Advanced Industrial Science and Technology (AIST)
  • Iwakabe Koichi
    Department of Chemical Engineering, Graduate School of Science and Engineering, Tokyo Institute of Technology
  • Takamatsu Takeichiro
    Professor Emeritus, Kyoto University
  • Nakaiwa Masaru
    Research Institute for Innovation in Sustainable Chemistry, National Institute of Advanced Industrial Science and Technology (AIST)

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With the aid of the McCabe–Thiele diagram, heuristic synthesis of an internally heat-integrated distillation column is addressed in this work. A new scheme for internal heat integration between a rectifying section and a stripping section is derived with the introduction of double-feed arrangement. The process configuration is characterized by its high thermodynamic efficiency and strong resilience to changes in operating conditions. Separation of a binary close-boiling mixture is conducted and the results obtained corroborate the advantages.

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