Simultaneous Injection-Effective Mixing Analysis of Palladium

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  • TESHIMA Norio
    Department of Applied Chemistry, Aichi Institute of Technology
  • NOGUCHI Daisuke
    Department of Applied Chemistry, Aichi Institute of Technology
  • JOICHI Yasutaka
    Graduate School of Natural Science and Technology, Okayama University
  • LENGHOR Narong
    Graduate School of Natural Science and Technology, Okayama University
  • OHNO Noriko
    Chemistry Laboratory, School of Business Administration, Asahi University
  • SAKAI Tadao
    Department of Applied Chemistry, Aichi Institute of Technology
  • MOTOMIZU Shoji
    Graduate School of Natural Science and Technology, Okayama University

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Abstract

A novel concept of simultaneous injection-effective mixing analysis (SIEMA) is proposed, and a SIEMA method applied to the spectrophotometric determination of palladium using a water-soluble chromogenic reagent has been demonstrated. The flow configuration of SIEMA is a hybrid format of flow injection analysis (FIA), sequential injection analysis (SIA) and multicommutation in flow-based analysis. Sample and reagent solutions are aspirated into each holding coil through each solenoid valve by a syringe pump, and then the zones are simultaneously dispensed (injected) into a mixing coil by reversed flow toward a detector through a confluence point. This results in effective mixing and rapid detection with low reagent consumption.

Journal

  • Analytical Sciences

    Analytical Sciences 26 (2), 143-144, 2010

    The Japan Society for Analytical Chemistry

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