Ruthenium-catalyzed Acylation of Arylpyridines with Acyl Chlorides via <i>ortho</i>-Selective C–H Bond Cleavage

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  • Takuya Kochi
    Department of Chemistry, Faculty of Science and Technology, Keio University
  • Aoi Tazawa
    Department of Chemistry, Faculty of Science and Technology, Keio University
  • Kazuki Honda
    Department of Chemistry, Faculty of Science and Technology, Keio University
  • Fumitoshi Kakiuchi
    Department of Chemistry, Faculty of Science and Technology, Keio University

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<jats:title>Abstract</jats:title> <jats:p>Ruthenium-catalyzed ortho-selective acylation of arylpyridines with acyl chlorides via C–H bond cleavage is described. Aromatic acyl chlorides as well as α,β-unsaturated acyl chlorides were coupled with arylpyridines to give aromatic ketones in the presence of [RuCl2(PPh3)3] as a catalyst and potassium carbonate as a base.</jats:p>

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  • Chemistry Letters

    Chemistry Letters 40 (9), 1018-1020, 2011-09

    Oxford University Press (OUP)

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