Selective Reduction of Carboxylic Acids to Aldehydes by a Ruthenium-catalyzed Reaction with 1,2-Bis(dimethylsilyl)benzene

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  • Konoka Miyamoto
    Department of Molecular and Materials Science, Graduate School of Engineering Sciences, Kyushu University
  • Yukihiro Motoyama
    Department of Molecular and Materials Science, Graduate School of Engineering Sciences, Kyushu University
  • Hideo Nagashima
    Department of Molecular and Materials Science, Graduate School of Engineering Sciences, Kyushu University

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<jats:title>Abstract</jats:title> <jats:p>Novel transformation of carboxylic acids to aldehydes is achieved by a one-pot procedure consisting of a ruthenium-catalyzed hydrosilane reduction with 1,2-bis(dimethylsilyl)benzene (2) followed by hydrolysis of the resulting cyclic disilylacetals 4.</jats:p>

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  • Chemistry Letters

    Chemistry Letters 41 (3), 229-231, 2012-02-18

    Oxford University Press (OUP)

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