Determination of Some Trace Metals by FAAS after Solid-phase Extraction with Amberlite XAD-1180/TAN Chelating Resin

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A new chelating resin was synthesized by immobilizing 1-(2-thiazolylazo)-2-naphthol through the –N=N– group on Amberlite XAD-1180. The resin was used for the preconcentration of Cd(II), Co(II), Cu(II), Mn(II), Ni(II), and Pb(II) ions and their determination by flame atomic absorption spectrometry (FAAS). The influences of some analytical parameters, such as the pH, volume of the sample, flow rates of the sample and eluent, matrix components, amount of the resin, and amount and type of the eluent on the recovery, were investigated. Those metals retained on the resin at pH 8.5 were eluted with 25 mL of 2 mol L<sup>−1</sup> HNO<sub>3</sub>. The sorption capacity of the resin was determined, except for Pb(II). The recoveries were found to be ≥95%, and the relative standard-deviation values were ≤4.3%. The detection limits were in the range of 0.1 – 3.6 μg L<sup>−1</sup>. For the accuracy of the method, the analysis of a certified reference material was performed. This method was applied to environmental water samples.

収録刊行物

  • Analytical sciences : the international journal of the Japan Society for Analytical Chemistry

    Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 28(5), 515-521, 2012-05-10

    The Japan Society for Analytical Chemistry

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各種コード

  • NII論文ID(NAID)
    10030757699
  • NII書誌ID(NCID)
    AA10500785
  • 本文言語コード
    ENG
  • 資料種別
    ART
  • ISSN
    09106340
  • NDL 記事登録ID
    023614037
  • NDL 請求記号
    Z54-F482
  • データ提供元
    CJP書誌  NDL  J-STAGE 
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