Effect of smear layer treatment on dentin bond of self-adhesive cements

  • KAMBARA Keisuke
    Cariology and Operative Dentistry, Department of Restorative Sciences, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University
  • NAKAJIMA Masatoshi
    Cariology and Operative Dentistry, Department of Restorative Sciences, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University
  • HOSAKA Keiichi
    Cariology and Operative Dentistry, Department of Restorative Sciences, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University
  • TAKAHASHI Masahiro
    Cariology and Operative Dentistry, Department of Restorative Sciences, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University
  • THANATVARAKORN Ornnicha
    Cariology and Operative Dentistry, Department of Restorative Sciences, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University Global Center of Excellence Program; International Research Center for Molecular Science in Tooth and Bone Diseases at Tokyo Medical and Dental University
  • ICHINOSE Shizuko
    Instrumental Analysis Research Center, Tokyo Medical and Dental University
  • M. FOXTON Richard
    Department of Conservative Dentistry, King's College London Dental Institute at Guy's, King's and St Thomas' Hospitals, King's College London
  • TAGAMI Junji
    Cariology and Operative Dentistry, Department of Restorative Sciences, Graduate School of Medical and Dental Sciences, Tokyo Medical and Dental University Global Center of Excellence Program; International Research Center for Molecular Science in Tooth and Bone Diseases at Tokyo Medical and Dental University

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Abstract

The purpose of this study was to compare the dentin bond strength of three self-adhesive cements with smear layer pretreatments using a calcium-chelating agent (EDTA) and deproteinizing solution (NaOCl) and to evaluate their interfacial characteristics. Smear layer-covered dentin surfaces were pretreated with EDTA for 60 s, NaOCl for 5 and 15 s, or none. Three self-adhesive cements; Clearfil SA luting (Kuraray Medical), Rely X Unicem clicker (3M ESPE) and Breeze (Pentron) were applied to the dentin surfaces. After 24-h water storage, shear bond strengths to dentin were determined. In addition, nanoleakage evaluation at the interface was performed using FE-SEM and EDS. EDTA-pretreatment significantly improved the bond strength of BR (p<0.05) and NaOCl-pretreatment for 15 s significantly improved the bond strength of RX (p<0.05). On the other hand, for SA, both pretreatments significantly decreased bond strength to dentin (p<0.05). Nanoleakage formation was observed in various amounts at the cement-dentin interfaces.

Journal

  • Dental Materials Journal

    Dental Materials Journal 31 (6), 980-987, 2012

    The Japanese Society for Dental Materials and Devices

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