Comprehensive Analytical Method for Semi-volatile Organic Compounds in Water Samples by Combination of Disk-type Solid-phase Extraction and Gas Chromatography–Mass Spectrometry Database System

• JINYA Daisuke

  Kitakyushu City Institute of Environmental Sciences

• IWAMURA Tomomi

  Kitakyushu City Institute of Environmental Sciences

• KADOKAMI Kiwao

  Faculty of Environmental Engineering, The University of Kitakyushu

Abstract

A disk-type solid-phase extraction method for simultaneous extraction of a wide range of semi-volatile organic compounds in water samples was developed. The developed method could extract 186 out of 202 model compounds from spiked environmental samples (0.1 μg/L) with 94% average recovery (50 – 111%). Compared with the previous cartridge-type method, the extraction time was reduced to approximately 1/6. Applying the combination of the developed method and the database system to environmental samples for non-target analyses, 39 micro-pollutants with a wide range of physicochemical properties were determined.

Journal

• Analytical Sciences

  Analytical Sciences 29 (4), 483-486, 2013

  The Japan Society for Analytical Chemistry

Keywords

• Analytical Chemistry

Details

• CRID: 1390282679238352000
• NII Article ID: 10031165343
• NII Book ID: AA10500785
• DOI: 10.2116/analsci.29.483
• COI: 1:STN:280:DC%2BC3srkt1ygsg%3D%3D
• ISSN: 13482246
• ISSN: 09106340
• NDL BIB ID: 024406636
• PubMed: 23574679
• Web Site: https://ndlsearch.ndl.go.jp/books/R000000004-I024406636
• Web Site: https://link.springer.com/content/pdf/10.2116/analsci.29.483.pdf
• Web Site: https://link.springer.com/article/10.2116/analsci.29.483/fulltext.html
• Web Site: https://www.jstage.jst.go.jp/article/analsci/29/4/29_483/_pdf
• Text Lang: en
• Data Source:
  • JaLC
  • NDL
  • Crossref
  • PubMed
  • CiNii Articles
  • KAKEN
• Abstract License Flag: Disallowed