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Reaction of benzo [b] furan with iodine azide gives in high yield a mixture of cis-and trans-2, 3-diazido-2, 3-dihydrobenzo [b] furans, both of which, upon treatment with alkali, are converted to 3-azidobenzo [b] furan. Similar reaction of 1-benzoyl-and 1-tosyl-indoles with iodine azide affords high yields of cis-and trans-1-benzoyl-and 1-tosyl-2, 3-diazidoindolines. Stereochemical assignment of the adducts is made on the basis of nuclear magnetic resonance spectroscopy.
収録刊行物
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- CHEMICAL & PHARMACEUTICAL BULLETIN
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CHEMICAL & PHARMACEUTICAL BULLETIN 26 (11), 3515-3520, 1978
公益社団法人 日本薬学会
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詳細情報 詳細情報について
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- CRID
- 1390001204168713856
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- NII論文ID
- 110003622906
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- NII書誌ID
- AA00602100
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- COI
- 1:CAS:528:DyaE1MXhsFWqs70%3D
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- ISSN
- 13475223
- 00092363
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- Crossref
- CiNii Articles
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- 抄録ライセンスフラグ
- 使用不可