熱イオン化検出器付ガスクロマトグラフィーによる覚せい剤の分析とその応用例について

• 山元 俊憲

• 寺田 賢

• 吉田 武美

• 吉村 三郎

• 黒岩 幸雄

書誌事項

タイトル別名

• Determination of Sympathomimetic Amine by Gas Chromatography equipped with Flame-Thermoionic Detector (FTD) and Its Application to Forensic Chemistry

抄録

Sympathomimetic amines, amphetamine and methamphetamine, were determined as trifluoroacetyl derivatives by gas chromatography (GC) equipped with a flame-thermionic detector (FTD). Resolution of these derivatives was carried out in a glass column (3 mm×1 m), packed with 1.5% SE-30 on Chromosorb W (AW-DMCS) at 110°C, with helium at a flow rate 50 ml/min. Detection limit of these amines was 0.1 ng. In a case of the autopsy samples from 4.5 month-postmortem suspected the intoxication of methamphetamine, we could detect the amine by FTD-GC, and the content was calculated to be 12.5 μg per g wet weight liver.

収録刊行物

• 衛生化学

  衛生化学 27 (5), 326-330, 1981

  公益社団法人 日本薬学会

キーワード

• amphetamine
• methamphetamine
• trifluoroacetyl derivative
• flame-thermionic detector
• gas chromatography
• autopsy sample
• mass spectrometry

詳細情報

• CRID: 1390001204496523776
• NII論文ID: 110003642896
• NII書誌ID: AN00021540
• DOI: 10.1248/jhs1956.27.326
• ISSN: 0013273X
• Web Site: http://www.jstage.jst.go.jp/article/jhs1956/27/5/27_5_326/_pdf
• Web Site: https://search.jamas.or.jp/link/ui/1982134836
• 本文言語コード: ja
• データソース種別:
  • JaLC
  • Crossref
  • CiNii Articles
• 抄録ライセンスフラグ: 使用不可