High-Resolution Electron Microscopic Observation of Microcrystalline Domains in an Amorphous Fe<SUB>84</SUB>B<SUB>16</SUB> Alloy

  • Hirotsu Yoshihiko
    Department of Mechanical Engineering, Technological University of Nagaoka
  • Akada Ryoji
    Department of Mechanical Engineering, Technological University of Nagaoka

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A high contrast bright-field lattice imaging method in high resolution transmission electron microscopy and its application to the observation of microcrystalline domains in a partially decomposed amorphous Fe84B16 alloy are described. A selection of an optimum defocus value was found to be necessary in obtaining dimensional information of the microcrystalline domains by lattice imaging. It is concluded that bcc-like microcrystals of Fe with a size of about 1 nm were already formed in an as-quenched Fe84B16 alloy and they gradually grew up to a size of about 2 nm on a low temperature annealing.

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詳細情報 詳細情報について

  • CRID
    1570854177335682944
  • NII論文ID
    110003929524
  • NII書誌ID
    AA10650595
  • 本文言語コード
    en
  • データソース種別
    • CiNii Articles

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