The Crystal Structure of m-Chlorobenzamide

• HATTORI Shigeaki

• TANIGUCHI Tomohiko

• KATO Yoshihiro

• SAKURAI Kiichi

書誌事項

タイトル別名

• Crystal Structure of m Chlorobenzamide

抄録

type:Article

The crystal structure of m-chlorobenzamide has been determined from three-dimensional X-ray data. Crystals are monoclinic, space group P2_1/a with a=9.87, b=4.76, c=15.85Ȧ, β=93.4°,z=4. A trial structure derived on the basis of isomorphism with m-iodobenzamide was refined by the block-diagonal least-squares method to R=0.108 for 1488 observed reflexions. The molecules are non-planar with an angle of 28.5° between the amide group and benzene ring. Pairs of molecules are each linked by NH…O hydrogen bonds (2.94Ȧ) across centres of symmetry to form dimers, and these dimers are further linked by NH…O hydrogen bonds (2.91Ȧ) into two-dimensional networks parallel to the c-plane.

収録刊行物

• 大阪教育大学紀要 第III部門 自然科学

  大阪教育大学紀要 第III部門 自然科学 24 (1), 35-42, 1975-10-04

  大阪教育大学

詳細情報

• CRID: 1390295414076558464
• NII論文ID: 110004068518
• NII書誌ID: AN00028200
• ISSN: 03737411
• DOI: 10.32287/td00010371
• NDL書誌ID: 1684871
• Web Site: http://ir.lib.osaka-kyoiku.ac.jp/dspace/handle/123456789/10371
• Web Site: https://ndlsearch.ndl.go.jp/books/R000000004-I1684871
• 本文言語コード: en
• データソース種別:
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  • IRDB
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  • CiNii Articles