Mechanical Properties of Dental Zirconia Ceramics Changed with Sandblasting and Heat Treatment

  • SATO Hideo
    Department of Biomaterials Science, Graduate School of Medical and Dental Sciences, Kagoshima University
  • YAMADA Kiyotaka
    Ceramic Physics Laboratory and Research Institute for Nanoscience, Kyoto Institute of Technology
  • PEZZOTTI Giuseppe
    Ceramic Physics Laboratory and Research Institute for Nanoscience, Kyoto Institute of Technology
  • NAWA Masahiro
    Central Research Laboratory, Matsushita Electric Works, Ltd.
  • BAN Seiji
    Department of Biomaterials Science, Graduate School of Medical and Dental Sciences, Kagoshima University

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  • Mechanical property of dental zirconia ceramics changed with sandblasting and heat treatment

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Abstract

Two types of tetragonal zirconia polycrystals (TZP), a ceria-stabilized TZP/Al2O3 nanocomposite (CZA) and a conventional yttria-stabilized TZP (Y-TZP), were sandblasted with 70-μm alumina and 125-μm SiC powders, then partially annealed at 500—1200°C for five minutes. Monoclinic ZrO2 content was determined by X-ray diffractometry and Raman spectroscopy. Biaxial flexure test was conducted on the specimens before and after the treatments. Monoclinic ZrO2 content and biaxial flexure strength increased after sandblasting, but decreased after heat treatment. However, in both cases, the strength of CZA was higher than that of Y-TZP. Raman spectroscopy showed that a compressive stress field was introduced on the sample surface after sandblasting. It was concluded that sandblasting induced tetragonal-to-monoclinic phase transformation and that the volume expansion associated with such a phase transformation gave rise to an increase in compressive stress on the surface of CZA. With the occurrence of such a strengthening mechanism in the microstructure, it was concluded that CZA was more susceptible to stress-induced transformation than Y-TZP.

Journal

  • Dental Materials Journal

    Dental Materials Journal 27 (3), 408-414, 2008

    The Japanese Society for Dental Materials and Devices

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