Effect of Delayed Application of the Dropped All-in-one Adhesives on Enamel and Dentin Bond Strengths

  • YAMADA Atsuko
    Department of Operative Dentistry, Field of Study of Biofunctional Recovery and Reconstruction, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Sciences
  • TAKABATAKE Yasumitsu
    Department of Operative Dentistry, Field of Study of Biofunctional Recovery and Reconstruction, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Sciences
  • YOSHIMITSU Keiko
    Department of Operative Dentistry, Field of Study of Biofunctional Recovery and Reconstruction, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Sciences
  • TANAKA Kumiko
    Department of Operative Dentistry, Field of Study of Biofunctional Recovery and Reconstruction, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Sciences
  • NOMOTO Masamori
    Department of Operative Dentistry, Field of Study of Biofunctional Recovery and Reconstruction, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Sciences
  • TASHIRO Yoko
    Department of Operative Dentistry, Field of Study of Biofunctional Recovery and Reconstruction, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Sciences
  • OMAE Masanori
    Department of Operative Dentistry, Field of Study of Biofunctional Recovery and Reconstruction, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Sciences
  • YAMAJI Kozo
    Department of Operative Dentistry, Field of Study of Biofunctional Recovery and Reconstruction, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Sciences
  • SHINNO Yasuo
    Department of Operative Dentistry, Field of Study of Biofunctional Recovery and Reconstruction, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Sciences
  • DOI Junichi
    Department of Operative Dentistry, Field of Study of Biofunctional Recovery and Reconstruction, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Sciences
  • NISHITANI Yoshihiro
    Department of Operative Dentistry, Field of Study of Biofunctional Recovery and Reconstruction, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Sciences
  • ITOTA Toshiyuki
    Department of Operative Dentistry, Field of Study of Biofunctional Recovery and Reconstruction, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Sciences
  • YOSHIYAMA Masahiro
    Department of Operative Dentistry, Field of Study of Biofunctional Recovery and Reconstruction, Okayama University Graduate School of Medicine, Dentistry and Pharmaceutical Sciences

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Other Title
  • ワンボトルワンステップ接着剤の採取後の放置時間が歯質接着性に及ぼす影響

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Abstract

The purpose of this study was to evaluate the effect of delayed application of the dropped all-in-one adhesives (Clearfil tri-S Bond and G-Bond) on enamel and dentin bond strengths. Human extracted premolars were used and flat enamel and dentin surfaces ground by 600-grit SiC paper were prepared. The tooth surfaces were treated with Clearfil tri-S Bond and G-Bond which were left for 0,5,10 and 30min after dropping of a adhesives on a shaded dish at constant temperature and humidity, and then covered with resin composites according to the manufacturers' instructions. After immersion in 37℃ water for 24 h, the teeth were serially sectioned into multiple slices and the micro-tensile bond strength was measured in a universal testing machine at a crosshead speed of 1.0mm/min. Data were statistically analyzed using one-way ANOVA and Dunnett's test at a significance level of 0.05. The weight changes of the dropped adhesives were also measured until 30 min under the shaded condition. In the comparison of the leaving time, a significant difference in the bond strength was only detected between 0 min and 30 min on enamel. The bond strength of Clearfil tri-S Bond to enamel after 30 min increased, but that of G-Bond after 30 min decreased (p<0.05). There was no significant difference in the bond strengths of Clearfil tri-S Bond and G-Bond to dentin. The weights of Clearfil tri-S Bond and G-Bond decreased with the leaving time after dropping and the percentage of the weights of adhesives were 82.7% for Clearfil tri-S Bond and 52.0% for G-Bond after 30min. These results suggested that the long-term leaving after dropping of the all-in-one adhesives affected the bond strengths to enamel bv evanoration of the solvents in adhesives.

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