A solution of the "intrinsic problem" of diastereomer method in chiral discrimination. Development of a method for highly efficient and sensitive discrimination of chiral alcohols

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  • A solution of the“intrinsic problem”of diastereomer method in chiral discrimination
  • solution of the intrinsic problem of diastereomer method in chiral discrimination Development of a method for highly efficient and sensitive discrimination of chiral alcohols
  • Development of a method for highly efficient and sensitive discrimination of chiral alcohols

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Very potent fluorescent chiral labeling reagents for alcohols, (R, R)-and (S, S)-2-(anthracene-2, 3-dicarboximido)cyclohexanecarboxylic acids, were developed. By labeling with them, the enantiomeric discriminations of primary alcohols having a methyl branching at the carbon from 2 to 9 by 1H-NMR and from 2 to 16 by HPLC were achieved. Further, HPLC separations of all four optical isomers of methyl branched secondary alcohols and enantiomers of 9-nonadecanol were also achieved.

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