Synthesis of (1<i>H</i>)-Isochromen-1-imines by Nickel-catalyzed Reaction of 2-Iodobenzamides with Alkynes

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  • Tomoya Miura
    Department of Synthetic Chemistry and Biological Chemistry, Kyoto University
  • Kentaro Hiraga
    Department of Synthetic Chemistry and Biological Chemistry, Kyoto University
  • Takeharu Toyoshima
    Department of Synthetic Chemistry and Biological Chemistry, Kyoto University
  • Motoshi Yamauchi
    Department of Synthetic Chemistry and Biological Chemistry, Kyoto University
  • Masahiro Murakami
    Department of Synthetic Chemistry and Biological Chemistry, Kyoto University

Abstract

<jats:title>Abstract</jats:title> <jats:p>2-Iodobenzamides reacted with alkynes in the presence of a nickel(0)/P(4-ClC6H4)3 catalyst to produce substituted (1H)-isochromen-1-imines. The reaction proceeded through the formation of an oxanickelacycle, alkyne insertion, and reductive elimination.</jats:p>

Journal

  • Chemistry Letters

    Chemistry Letters 41 (8), 798-800, 2012-07-28

    Oxford University Press (OUP)

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