Facile Synthesis of Nitrogen-containing Polycyclic Aromatic Hydrocarbons from Perylene Bisimides

DOI PDF 被引用文献2件 参考文献23件
  • Satoru Ito
    Department of Applied Chemistry, Graduate School of Engineering, Nagoya University
  • Satoru Hiroto
    Department of Applied Chemistry, Graduate School of Engineering, Nagoya University
  • Hiroshi Shinokubo
    Department of Applied Chemistry, Graduate School of Engineering, Nagoya University

抄録

<jats:title>Abstract</jats:title> <jats:p>We have developed a facile procedure for the synthesis of π-extended fluorubins from perylene bisimides. Iridium-catalyzed direct borylation, the Suzuki–Miyaura cross-coupling, and an acid-condensation sequence afforded π-extended fluorubins 1 in moderate yields. X-ray diffraction analysis revealed a planar structure of 1. In addition, optical analysis and DFT calculations indicated the presence of intramolecular charge-transfer interactions in 1c.</jats:p>

収録刊行物

  • Chemistry Letters

    Chemistry Letters 43 (8), 1309-1311, 2014-05-14

    Oxford University Press (OUP)

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