Effect of facing annealing on crystallization and decomposition of Pb(Mg₁/₃Nb₂/₃)O₃ thin films prepared by CSD technique using MOD solution
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- Effect of facing annealing on crystallization and decomposition of Pb(Mg<sub>1/3</sub>Nb<sub>2/3</sub>)O<sub>3</sub> thin films prepared by CSD technique using MOD solution
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This study examined improvement of the crystallinity and the decomposition mechanism for the Pb(Mg1/3Nb2/3)O3 (PMN) thin films using chemical solution deposition (CSD) technique with a metallo-organic decomposition (MOD) solution. The PMN thin film crystallinity increases with higher annealing temperature, but improvement is slight at temperatures higher than 700°C. The facing annealing has a distinct effect on the crystallinity of PMN thin film at 650°C, which is the lowest annealing temperature examined in this study. The ratio of the pyrochlore phase has a peak at 750°C with or without the facing annealing. The facing annealing also has a distinct effect on PMN thin film decomposition at 800°C. Improvement of the crystallinity and of the homogeneity of the morphology of PMN thin films deposited at 650°C was possible under the facing condition. The decomposition occurs locally, and the residual PMN region has high crystallinity and stoichiometry. The atomic structure of the PMN lattice has a fluctuation that is characteristic in the relaxor, which is related to the polar-nano region (PNR). The chemically ordered region (COR) also appears in PMN even at a lower annealing temperature than that of bulk relaxor materials.
収録刊行物
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- Journal of the Ceramic Society of Japan
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Journal of the Ceramic Society of Japan 121 (1411), 326-326, 2013
公益社団法人 日本セラミックス協会
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詳細情報 詳細情報について
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- CRID
- 1390001205286890496
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- NII論文ID
- 130004950808
- 130004950819
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- NII書誌ID
- AA12229489
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- ISSN
- 13486535
- 18820743
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- NDL書誌ID
- 024223734
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- NDL
- Crossref
- CiNii Articles
- KAKEN
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- 抄録ライセンスフラグ
- 使用不可