Highlighted Paper selected by Editor-in-Chief : Asymmetric Total Syntheses and Structure Elucidations of (+)-Eurotiumide F and (+)-Eurotiumide G

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  • Nakayama Atsushi
    Graduate School of Pharmaceutical Sciences, Tokushima University
  • Sato Hideo
    Graduate School of Pharmaceutical Sciences, Tokushima University
  • Nagano Shuji
    Graduate School of Pharmaceutical Sciences, Tokushima University
  • Karanjit Sangita
    Graduate School of Pharmaceutical Sciences, Tokushima University
  • Imagawa Hiroshi
    Faculty of Pharmaceutical Sciences, Tokushima Bunri University
  • Namba Kosuke
    Graduate School of Pharmaceutical Sciences, Tokushima University

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  • Asymmetric Total Syntheses and Structure Elucidations of (+)-Eurotiumide F and (+)-Eurotiumide G

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<p>Asymmetric total syntheses of dihydropyran containing natural products, (+)-eurotiumide F and (+)-eurotiumide G have been described. These total syntheses revealed the absolute configuration of eurotiumide F and G, and confirmed the reported structure of eurotiumide F and revised the reported structure of eurotiumide G. Highlight of these syntheses is thermal rearrangement with 4-methoxyisochroman-1-one derivative having propargyl ether on phenolic ether under thermal condition to construct dihydropyran ring. X-Ray crystallographic analysis of (+)-eurotiumide G clarified the stereochemistry at the C1-position.</p>

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