Browning, Starch Gelatinization, Water Sorption, Glass Transition, and Caking Properties of Freeze-dried Maca (Lepidium meyenii Walpers) Powders

  • Granados Alex Eduardo Alvino
    Graduate School of Biosphere Science, Hiroshima University
  • Kawai Kiyoshi
    Graduate School of Biosphere Science, Hiroshima University Graduate School of Integrated Sciences for Life, Hiroshima University

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  • Browning, Starch Gelatinization, Water Sorption, Glass Transition, and Caking Properties of Freeze-dried Maca (<i>Lepidium meyenii</i> Walpers) Powders

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<p>The browning, gelatinization of starch, water sorption, glass transition, and caking properties of freeze-dried maca (Lepidium meyenii Walpers) powders were investigated and compared with a commercial maca powder. The freeze-dried maca powders had lower optical density (browning) and higher enthalpy change for starch gelatinization than the commercial maca. This resulted from a difference in thermal history. The equilibrium water contents of the freeze-dried maca powders were higher than those of commercial maca at each water activity (aw) because of differences in amorphous part. The glass transition temperature (Tg) was evaluated by differential scanning calorimetry. There was a negligible difference in the anhydrous Tg (79.5–80.2 ºC) among the samples. The Tg-depression of freeze-dried maca powders induced by water sorption was more gradual than that of the commercial maca due to a difference in water insoluble material content. From the results, critical water activity (awc) was determined as the aw at which Tg becomes 25 ºC. There was negligible caking below aw = 0.328. At higher aw, the degree of caking remarkably increased with a large variation depending on the samples. The degree of caking could be described uniformly as a function of aw/awc. From these results, we propose an empirical approach to predict the caking of maca powders.</p>

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