Chemical synthesis of cellulose derivatives by a convergent synthetic method 合流型合成法によるセルロース誘導体の化学合成

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Author

    • 西村, 健 ニシムラ, タケシ

Bibliographic Information

Title

Chemical synthesis of cellulose derivatives by a convergent synthetic method

Other Title

合流型合成法によるセルロース誘導体の化学合成

Author

西村, 健

Author(Another name)

ニシムラ, タケシ

University

京都大学

Types of degree

博士 (農学)

Grant ID

甲第6455号

Degree year

1996-03-23

Note and Description

博士論文

Table of Contents

  1. 論文目録 / (0001.jp2)
  2. CONTENTS / p1 (0004.jp2)
  3. LIST OF FIGURES / p3 (0005.jp2)
  4. LIST OF TABLES / p5 (0006.jp2)
  5. INTRODUCTION / p1 (0007.jp2)
  6. Chapter 1 Selection and Syntheses of Starting Materials for the Convergent Synthesis / p4 (0009.jp2)
  7. 1-1 Basic synthetic design for cellulose / p6 (0010.jp2)
  8. 1-2 Selection of glycosylation method / p8 (0011.jp2)
  9. 1-3 Selection of possible starting materials(2-6)for the convergent synthesis of cellulose / p10 (0012.jp2)
  10. 1-4 Preparation of possible starting materials(2-6) / p12 (0013.jp2)
  11. 1-5 Preparation of glycosyl donors(2c-6c) and acceptors(2a-6a) / p14 (0014.jp2)
  12. 1-6 Glycosylation between glycosyl donors (2c-6c) and glycosyl acceptors (2a-6a) / p15 (0014.jp2)
  13. Summary / p19 (0016.jp2)
  14. Chapter 2 Synthesis of Cellotetraose / p21 (0017.jp2)
  15. 2-1 Preparation of cellobiose glycosyl donors(13,19)and acceptor 11 / p22 (0018.jp2)
  16. 2-2 Side reactions of glycosyl imidate during the boron trifluoride etherate catalyzed glycosylation / p23 (0018.jp2)
  17. 2-3 Use of acetyl group as temporary protective group at O-4' position / p27 (0020.jp2)
  18. 2-4 Glycosylation / p29 (0021.jp2)
  19. 2-5 Deprotection / p30 (0022.jp2)
  20. 2-6 Summary / p33 (0023.jp2)
  21. Chapter 3 Synthesis of Cellooctaose / p35 (0024.jp2)
  22. 3-1 Preparation of a cellotclraose glycosyl donor 26 and acceptor 28 / p35 (0024.jp2)
  23. 3-2 Glycosylation using high vacuum system / p37 (0025.jp2)
  24. 3-3 Deprotection / p40 (0027.jp2)
  25. 3-4 Summary / p42 (0028.jp2)
  26. Chapter 4 First Syntheses of Celloeicosaose Derivatives and Their Some Properties / p44 (0029.jp2)
  27. 4-1 Convergent synthesis of a celloeicosaose derivative 48 / p44 (0029.jp2)
  28. Preparation of glycosyl acceptor / p47 (0030.jp2)
  29. Glycosylation / p47 (0030.jp2)
  30. 4-2 Deprotcction / p52 (0033.jp2)
  31. 4-3 Some properties of synthesized cellulose homologous series NMR spectra / p54 (0034.jp2)
  32. Gel Permeation Chromatography (GPC)analysis / p54 (0034.jp2)
  33. Optical rotation / p57 (0035.jp2)
  34. 4-4 Summary / p61 (0037.jp2)
  35. CONCLUSIONS / p63 (0038.jp2)
  36. EXPERIMENTAL / p67 (0040.jp2)
  37. LIST OF REFERENCES / p93 (0053.jp2)
  38. PUBLICATIONS / p99 (0056.jp2)
  39. ACKNOWLEDGEMENT / p100 (0057.jp2)
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Codes

  • NII Article ID (NAID)
    500000131179
  • NII Author ID (NRID)
    • 8000000965868
  • DOI(NDL)
  • NDLBibID
    • 000000295493
  • Source
    • NDL ONLINE
    • NDL Digital Collections

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