Development of a liquid-liquid-solid phase-transfer-catalyzed derivatization method for the microanalysis of aqueous compounds and Its applications in forensic toxicology 水溶性化合物の微量分析のための液-液-固相間移動誘導体化法の開発とその法薬毒物学分野における応用

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著者
    • 三木, 昭宏 ミキ, アキヒロ
書誌事項
タイトル

Development of a liquid-liquid-solid phase-transfer-catalyzed derivatization method for the microanalysis of aqueous compounds and Its applications in forensic toxicology

タイトル別名

水溶性化合物の微量分析のための液-液-固相間移動誘導体化法の開発とその法薬毒物学分野における応用

著者名

三木, 昭宏

著者別名

ミキ, アキヒロ

学位授与大学

同志社大学

取得学位

博士 (工学)

学位授与番号

乙第171号

学位授与年月日

1999-01-29

注記・抄録

博士論文

目次
  1. Contents / p2 (0003.jp2)
  2. Preface / p1 (0004.jp2)
  3. References / p5 (0006.jp2)
  4. Chapter 1 Basic Study for the Application of Liquid-Liquid-Solid Phase-Transfer Catalysis to the Extractive Derivatization of Anionic Compounds / p7 (0007.jp2)
  5. A.Application of Phase-Transfer Catalysis in Analytical Chemistry: A Background Summary / p7 (0007.jp2)
  6. B.Adaptation of Liquid-Liquid-Solid Phase-Transfer Catalysis to the Extractive Derivatization of Trace-Level Anionic Compounds / p12 (0010.jp2)
  7. Introduction / p12 (0010.jp2)
  8. Results and Discussion / p13 (0010.jp2)
  9. Conclusion / p29 (0018.jp2)
  10. Experimental / p30 (0019.jp2)
  11. References / p33 (0020.jp2)
  12. Chapter 2 Systematic Analysis of Dialkyl Phosphates,the Primary Degradation Products of Organophosphorus Pesticides,via Triphasal Pentafluorobenzylation / p36 (0022.jp2)
  13. Introduction / p36 (0022.jp2)
  14. Results and Discussion / p39 (0023.jp2)
  15. Conclusion / p51 (0029.jp2)
  16. Experimental / p51 (0029.jp2)
  17. References / p55 (0031.jp2)
  18. Chapter 3 Determination of Typical Carboxylate-Type Agrochemicals, Fluoroacetic Acid and Phenoxy Acid Herbicides,via Triphasal Pentafluorobenzylation / p56 (0032.jp2)
  19. Introduction / p56 (0032.jp2)
  20. Results and Discussion / p58 (0033.jp2)
  21. Conclusion / p71 (0039.jp2)
  22. Experimental / p71 (0039.jp2)
  23. References / p73 (0040.jp2)
  24. Chapter 4 Application of Triphasal Pentafluorobenzylation for the Microanalysis of Inorganic Anions of Toxicological Interest / p75 (0041.jp2)
  25. A.Determination of Sulfide in Blood / p75 (0041.jp2)
  26. Introduction / p75 (0041.jp2)
  27. Results and Discussion / p76 (0042.jp2)
  28. Conclusion / p82 (0045.jp2)
  29. B.Simultaneous Determination of Cyanide and Thiocyanate / p83 (0045.jp2)
  30. Introduction / p83 (0045.jp2)
  31. Results and Discussion / p85 (0046.jp2)
  32. Conclusion / p94 (0051.jp2)
  33. Experimental / p95 (0051.jp2)
  34. References / p98 (0053.jp2)
  35. Chapter 5 Trace Determination of Alkyl Methylphosphonates,the Main Metabolites and Degradation Products of Organo-phosphorus Nerve Agents,via Triphasal Pentafluorobenzylation / p100 (0054.jp2)
  36. A.Conditional Settings for the Triphasal Derivatization and the Comparison of This Method with Anhydrous Derivatization / p100 (0054.jp2)
  37. Introduction / p100 (0054.jp2)
  38. Results and Discussion / p103 (0055.jp2)
  39. Conclusion / p109 (0058.jp2)
  40. B.Analysis of Biological and Environmental Samples / p110 (0059.jp2)
  41. Introduction / p110 (0059.jp2)
  42. Results and Discussion / p110 (0059.jp2)
  43. Conclusion / p121 (0064.jp2)
  44. Experimental / p122 (0065.jp2)
  45. References / p126 (0067.jp2)
  46. Closing Statements / p128 (0068.jp2)
  47. List of Publications / p131 (0069.jp2)
  48. Acknowledgements / p136 (0072.jp2)
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各種コード
  • NII論文ID(NAID)
    500000168306
  • NII著者ID(NRID)
    • 8000000168578
  • DOI(NDL)
  • NDL書誌ID
    • 000000332620
  • データ提供元
    • NDL ONLINE
    • NDLデジタルコレクション
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