Development of a liquid-liquid-solid phase-transfer-catalyzed derivatization method for the microanalysis of aqueous compounds and Its applications in forensic toxicology 水溶性化合物の微量分析のための液-液-固相間移動誘導体化法の開発とその法薬毒物学分野における応用
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Bibliographic Information
- Title
-
Development of a liquid-liquid-solid phase-transfer-catalyzed derivatization method for the microanalysis of aqueous compounds and Its applications in forensic toxicology
- Other Title
-
水溶性化合物の微量分析のための液-液-固相間移動誘導体化法の開発とその法薬毒物学分野における応用
- Author
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三木, 昭宏
- Author(Another name)
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ミキ, アキヒロ
- University
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同志社大学
- Types of degree
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博士 (工学)
- Grant ID
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乙第171号
- Degree year
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1999-01-29
Note and Description
博士論文
Table of Contents
- Contents / p2 (0003.jp2)
- Preface / p1 (0004.jp2)
- References / p5 (0006.jp2)
- Chapter 1 Basic Study for the Application of Liquid-Liquid-Solid Phase-Transfer Catalysis to the Extractive Derivatization of Anionic Compounds / p7 (0007.jp2)
- A.Application of Phase-Transfer Catalysis in Analytical Chemistry: A Background Summary / p7 (0007.jp2)
- B.Adaptation of Liquid-Liquid-Solid Phase-Transfer Catalysis to the Extractive Derivatization of Trace-Level Anionic Compounds / p12 (0010.jp2)
- Introduction / p12 (0010.jp2)
- Results and Discussion / p13 (0010.jp2)
- Conclusion / p29 (0018.jp2)
- Experimental / p30 (0019.jp2)
- References / p33 (0020.jp2)
- Chapter 2 Systematic Analysis of Dialkyl Phosphates,the Primary Degradation Products of Organophosphorus Pesticides,via Triphasal Pentafluorobenzylation / p36 (0022.jp2)
- Introduction / p36 (0022.jp2)
- Results and Discussion / p39 (0023.jp2)
- Conclusion / p51 (0029.jp2)
- Experimental / p51 (0029.jp2)
- References / p55 (0031.jp2)
- Chapter 3 Determination of Typical Carboxylate-Type Agrochemicals, Fluoroacetic Acid and Phenoxy Acid Herbicides,via Triphasal Pentafluorobenzylation / p56 (0032.jp2)
- Introduction / p56 (0032.jp2)
- Results and Discussion / p58 (0033.jp2)
- Conclusion / p71 (0039.jp2)
- Experimental / p71 (0039.jp2)
- References / p73 (0040.jp2)
- Chapter 4 Application of Triphasal Pentafluorobenzylation for the Microanalysis of Inorganic Anions of Toxicological Interest / p75 (0041.jp2)
- A.Determination of Sulfide in Blood / p75 (0041.jp2)
- Introduction / p75 (0041.jp2)
- Results and Discussion / p76 (0042.jp2)
- Conclusion / p82 (0045.jp2)
- B.Simultaneous Determination of Cyanide and Thiocyanate / p83 (0045.jp2)
- Introduction / p83 (0045.jp2)
- Results and Discussion / p85 (0046.jp2)
- Conclusion / p94 (0051.jp2)
- Experimental / p95 (0051.jp2)
- References / p98 (0053.jp2)
- Chapter 5 Trace Determination of Alkyl Methylphosphonates,the Main Metabolites and Degradation Products of Organo-phosphorus Nerve Agents,via Triphasal Pentafluorobenzylation / p100 (0054.jp2)
- A.Conditional Settings for the Triphasal Derivatization and the Comparison of This Method with Anhydrous Derivatization / p100 (0054.jp2)
- Introduction / p100 (0054.jp2)
- Results and Discussion / p103 (0055.jp2)
- Conclusion / p109 (0058.jp2)
- B.Analysis of Biological and Environmental Samples / p110 (0059.jp2)
- Introduction / p110 (0059.jp2)
- Results and Discussion / p110 (0059.jp2)
- Conclusion / p121 (0064.jp2)
- Experimental / p122 (0065.jp2)
- References / p126 (0067.jp2)
- Closing Statements / p128 (0068.jp2)
- List of Publications / p131 (0069.jp2)
- Acknowledgements / p136 (0072.jp2)