Development of a selective homonuclear dipolar recoupling method in magic-angle spinning solid-state NMR and its application to the structural analysis of a molecule マジック角度回転固体NMRにおける同種核間双極子相互作用の選択的復活法の開発と分子の構造解析への応用

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Title: Development of a selective homonuclear dipolar recoupling method in magic-angle spinning solid-state NMR and its application to the structural analysis of a molecule

博士論文

論文目録 / (0001.jp2)
Contents / p1 (0005.jp2)
Abstruct / p4 (0008.jp2)
1 Introduction / p6 (0010.jp2)
2 NMR Spectra of Homonuclear Spin-1/2 Pairs Dipolar-Recoupled by Radio-Frequency Field Irradiation under Magic-Angle Spinning / p11 (0015.jp2)
2.1 Introduction / p11 (0015.jp2)
2.2 Theory / p14 (0018.jp2)
2.3 Results and discussion / p37 (0041.jp2)
2.4 Conclusion / p45 (0049.jp2)
Appendix1 Line splitting of the powder line shapes / p48 (0052.jp2)
3 Selective Homonuclear Polarization Transfer in the Tilted Rotating Frame under Magic Angle Spinning in Solids / p58 (0072.jp2)
3.1 Introduction / p58 (0072.jp2)
3.2 Theory / p61 (0075.jp2)
3.3 Experimental results and discussion / p69 (0083.jp2)
3.4 Conclusion / p79 (0093.jp2)
4 Determination of the Complete Structure of a Uniformly Labeled Molecule by Rotational Resonance Solid-State NMR in the Tilted Rotating Frame / p84 (0108.jp2)
4.1 Introduction / p84 (0108.jp2)
4.2 Method of Structure Determination / p86 (0110.jp2)
4.3 Experimental results and discussion / p89 (0113.jp2)
4.4 Conclusion / p103 (0127.jp2)
References / p110 (0147.jp2)
Acknowledgements / p118 (0155.jp2)
Frequency Response Method for Study of Kinetic Details of a Heterogeneous Catalytic Reaction of Gases.2.A Methanol Conversion to Olefins / p3319 (0187.jp2)

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