Determination of the absolute configurations of linear polyols by means of NMR chiral anisotropic reagents, 2ATMA and MTPA
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著者
書誌事項
- タイトル
-
Determination of the absolute configurations of linear polyols by means of NMR chiral anisotropic reagents, 2ATMA and MTPA
- 著者名
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幸田, 恭治
- 著者別名
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コウダ, キョウジ
- 学位授与大学
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徳島大学
- 取得学位
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博士 (薬学)
- 学位授与番号
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甲第1080号
- 学位授与年月日
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2000-03-26
注記・抄録
博士論文
目次
- 論文目録 / (0003.jp2)
- 論文内容要旨 / (0004.jp2)
- CONTENTS / (0008.jp2)
- CHAPTER I INTRODUCTION / p1 (0009.jp2)
- CHAPTER II NOVEL CHIRAL ANISOTROPIC REAGENTS,2ATMA AND 9ATMA,FOR ABSOLUTE CONFIGURATION DETERMINATION OF CHIRAL SECONDARY ALCOHOLS / p3 (0010.jp2)
- II-a.Introduction / p3 (0010.jp2)
- II-b.Synthesis and Resolution of 2-Anthryl-methoxyacetic Acid / p8 (0013.jp2)
- II-c.Application of 2ATMA to Secondary Alcohols / p14 (0016.jp2)
- II-d.An Improved Synthesis of 9-Anthryl-methoxyacetic acid / p20 (0019.jp2)
- II-e.Application of 9ATMA to a γ-Chiral Primary Alcohol / p23 (0020.jp2)
- CHAPTER III DETERMINATION OF THE ABSOLUTE CONFIGURATION OF TAUROLIPID B / p25 (0021.jp2)
- III-a.Introduction / p25 (0021.jp2)
- III-b.Determination of the Absolute Configuration / p26 (0022.jp2)
- III-c.Investigation of Di-2ATMA Ester / p31 (0024.jp2)
- III-d.Application of the Modified Mosher's Method / p33 (0025.jp2)
- III-e.Confirmation by CD Exciton Chirality Method / p36 (0027.jp2)
- CHAPTER IV APPLICATION OF THE MODIFIED MOSHER'S METHOD TO LINEAR 1,3-DIOLS / p39 (0028.jp2)
- IV-a.Introduction / p39 (0028.jp2)
- IV-b.Preparation of Mono-MTPA esters with Various Linear 1,3-Diols / p39 (0028.jp2)
- IV-c.Determination of Relative Configuration / p41 (0029.jp2)
- IV-d.Determination of the Absolute Configuration by use of CD Exciton Chirality Method / p41 (0029.jp2)
- IV-e.Application of the Modified Mosher's Method / p42 (0030.jp2)
- IV-f.Conclusion / p44 (0031.jp2)
- IV-g.Addendum / p44 (0031.jp2)
- CHAPTER V EXPERIMENTAL SECTION / p47 (0032.jp2)
- ACKNOWLEDGMENTS / p87 (0052.jp2)
- REFERENCES AND NOTES / p89 (0053.jp2)