Compendium of organic synthetic methods

Author(s)

• Harrison, Ian T.
• Harrison, Shuyen
• Wade, L. G.
• Smith, Michael B.
• Hegedus, Louis S.

Bibliographic Information

Compendium of organic synthetic methods

Ian T. Harrison and Shuyen Harrison

（A Wiley-Interscience publication）

Wiley, c1971-

• [v. 1]
• v. 2
• v. 3
• v. 4
• v. 5
• v. 6
• v. 7
• v. 8
• v. 9
• v. 10
• v. 11
• v. 12
• v. 13

Note

[Vol. 1]-Vol. 2. by Ian T. Harrison and Shuyen Harrison

Vol. 3. by Louis S. Hegedus and Leroy Wade

Vol. 4-Vol. 5. by Leroy G. Wade, Jr

Vol. 6- by Michael B. Smith

Description and Table of Contents

Volume

v. 4 ISBN 9780471049234

Description

Compendium of Organic Synthetic Methods Volume III Louis S. Hegedus& Leroy G. Wade, Jr. Presents the new synthetic methods forpreparation of monofunctional compounds for 1974, 1975, and 1976.Sections correspond to most of the possible interconversionsbetween the major functional groups. In addition, the volumecontains examples of new methods of preparation of difunctionalcompounds formed from pairs of the major functional groups. 1977 (0471-36752-4) 495 pages Compendium of Organic Synthetic MethodsVolume II Ian T. Harrison & Shuyen Harrison ". a valuablesupplement to their earlier volume. Not only does it contain manyadditional examples of methods of preparing monofunctionalcompounds, but it also contains a new section covering preparationof difunctional compounds.. particularly useful for the syntheticorganic chemist who wishes to locate fairly quickly a recipe for asimple functional group transformation." --Laboratory Practice 1974(0 471-35551-8) 437 pages Compendium of Organic Synthetic MethodsVolume I Ian T. Harrison & Shuyen Harrison A compilation oforganic functional group transformations, including 3000 syntheticmethods presented in the form of reactions with leading references.Divided into sections corresponding to all possibleinterconversions between the major functional groups: acetylene,carboxylic acid, alcohol, etc. Other parts deal with the protectionof carboxylic acids, alcohols, aldehydes, amines, and ketones. "Avery usable volume . deserves a Wide sale." --Journal of theAmerican Chemical Society 1971 (0 471-35550-X) 529 pages

Table of Contents

Abbreviations. Index, Monofunctional Compounds. Index, Difunctional Compounds. Introduction. Preparation of Acetylenes. Preparation of Carboxylic Acids, Acid Halides, andAnhydrides. Preparation of Alcohols and Phenols. Preparation of Aldehydes. Preparation of Alkyls, Methylenes, and Aryls. Preparation of Amides. Preparation of Amines. Preparation of Esters. Preparation of Ethers and Epoxides. Preparation of Halides and Sulfonates. Preparation of Hydrides. Preparation of Ketones. Preparation of Nitriles. Preparation of Olefins. Preparation of Difunctional Compounds.

Volume

v. 9 ISBN 9780471145790

Description

Organic transformations are the heart of synthetic organic chemistry. The Compendium of Organic Synthetic Methods series facilitates the search for the most useful functional group transformations in organic chemistry. Compendium of Organic Synthetic Methods, Volume 9, provides quick access to proven protocols for the newest, most useful reactions and transformations. It contains both functional group transformations and bond-forming reactions, and focuses on the use of reagents readily available or easily prepared and handled in the laboratory. This valuable desktop resource contains over 1,200 examples of published reactions for the preparation of monofunctional compounds in a handy reference, as well as over 800 examples of difunctional compounds, and features over 30 more reviews than Volume 8. As in all the previous Compendium volumes, the classification schemes used allow for quick and easy reference and information retrieval. Chemical transformations are classified by the reacting functional group of the starting material and then by the functional group formed. Helpful indices are provided for both monofunctional and difunctional compounds as an efficient means of guidance to specific classes of transformations. Compendium of Organic Synthetic Methods, Volume 9, is an unparalleled source of information on the methods, reactions, and transformations in contemporary organic chemistry for the working chemist and student. Volume 9 in the series originated by I. T. Harrison and S. Harrison

Table of Contents

Preparation of Alkynes. Preparation of Acid Derivatives. Preparation of Alcohols. Preparation of Aldehydes. Preparation of Alkyls, Methylenes and Aryls. Preparation of Amides. Preparation of Amines. Preparation of Esters. Preparation of Ethers, Epoxides and Thioethers. Preparation of Halides and Sulfonates. Preparation of Hydrides. Preparation of Ketones. Preparation of Nitriles. Preparation of Alkenes. Preparation of Oxides. Preparation of Difunctional Compounds. Author Index.

Volume

v. 10 ISBN 9780471202011

Description

Compendium of Organic Synthetic Methods continues the motivation of the series, which is to facilitate the search for quality, selected functional group transformations, organized by reacting functional group of starting material and functional group formed, with full references to each reaction.

Table of Contents

Preface. Abbreviations. Index, Monofunctional Compounds. Index, Difunctional Compounds. Introduction. 1. Preparation of Alkynes. 2. Preparation of Acid Derivatives and Anhydrides. 3. Preparation of Alcohols. 4. Preparation of Aldehydes. 5. Preparation of Alkyls, Methylenes and Aryls. 6. Preparation of Amides. 7. Preparation of Amines. 8. Preparation of Esters. 9. Preparation of Ethers, Epoxides and Thioethers. 10. Preparation of Halides and Sulfonates. 11. Preparation of Hydrides. 12. Preparation of Ketones. 13. Preparation of Nitriles. 14. Preparation of Alkenes. 15. Preparation of Oxides. 16. Preparation of Difunctional Compounds. Author Index.

Volume

v. 11 ISBN 9780471259657

Description

Compendium of Organic Synthetic Methods, Volume 11 continues the motivation of the series, which is to facilitate the search for quality, selected functional group transformations, organized by reacting functional group of starting material and functional group formed, with full references to each reaction.

Table of Contents

Preface. Abbreviations. Index, Monofunctional Compounds. Index, Difunctional Compounds. Introduction. 1. Preparation of Alkynes. 2. Preparation of Acid Derivatives and Anhydrides. 3. Preparation of Alcohols. 4. Preparation of Aldehydes. 5. Preparation of Alkyls, Methylenes and Aryls. 6. Preparation of Amides. 7. Preparation of Amines. 8. Preparation of Esters. 9. Preparation of Ethers, Epoxides and Thioethers. 10 . Preparation of Halides and Sulfonates. 11. Preparation of Hydrides. 12. Preparation of Ketones. 13. Preparation of Nitriles. 14. Preparation of Alkenes. 15. Preparation of Oxides. 16. Preparation of Difunctional Compounds. Author Index.

Volume

[v. 1] ISBN 9780471355502

Description

Provides synthetic chemists with a method for rapid retrieval of information from the literature, listing material by reaction type rather than by author name or publication date. Each updated volume presents the latest synthetic methods for preparation of monofunctional and difunctional compounds. The organization is logical and easy to follow; sections are arranged according to the possible interconversions between the major functional groups. Enables synthetic chemists to keep abreast of recent developments and retrieve a specific piece of information quickly and easily.

Table of Contents

ABBREVIATIONS ix INDEX xi INTRODUCTION xiii 1 PREPARATION OF ACETYLENES 1 2 PREPARATION OF CARBOXYLIC ACIDS, ACID HALIDES, AND ANHYDRIDES 16 3 PREPARATION OF ALCOHOLS AND PHENOLS 75 4 PREPARATION OF ALDEHYDES 132 5 PREPARATION OF ALKYLS, METHYLENES, AND ARYLS 177 6 PREPARATION OF AMIDES 203 7 PREPARATION OF AMINES 8 PREPARATION OF ESTERS 271 9 PREPARATION OF ETHERS AND EPOXIDES 309 10 PREPARATION OF HALIDES AND SULFONATES 329 11 PREPARATION OF HYDRIDES 375 12 PREPARATION OF KETONES 379 13 PREPARATION OF NITRILES 457 14 PREPARATION OF OLEFINS 479

Volume

v. 2 ISBN 9780471355519

Description

Provides synthetic chemists with a method for rapid retrieval of information from the literature, listing material by reaction type rather than by author name or publication date. Each updated volume presents the latest synthetic methods for preparation of monofunctional and difunctional compounds. The organization is logical and easy to follow; sections are arranged according to the possible interconversions between the major functional groups. Enables synthetic chemists to keep abreast of recent developments and retrieve a specific piece of information quickly and easily.

Table of Contents

Abbreviations vii Index, Monofunctional compounds ix Index, Difunctional compounds xi How to use the compendium xiii Introduction xv 1 Preparation of acetylenes 1 2 Preparation of carboxylic acids, acid halides, and anhydrides 7 3 Preparation of alcohols and phenols 28 4 Preparation of aldehydes 53 5 Preparation of alkyls, methylenes, and aryls 70 6 Preparation of amides 82 7 Preparation of amines 92 8 Preparation of esters 108 9 Preparation of ethers and epoxides 127 10 Preparation of halides and sulfonates 136 11 Preparation of hydrides 146 12 Preparation of ketones 155 13 Preparation of nitriles 185 14 Preparation of olefins 193 15 Preparation of difunctional compounds 214

Volume

v. 3 ISBN 9780471367529

Description

Compendium of Organic Synthetic Methods, Vols. I & II By Ian T.Harrison & Shuyen Harrison Volume I A complete one-volumecompilation of organic functional group transformations. Includes3000 synthetic methods presented in the form of reactions withleading references. Divided into sections corresponding to allpossible interconversions between the major functional groups:acetylene, carboxylic acid, alcohol, aldehyde, etc. Other partsdeal with the protection of carboxylic acids, alcohols, aldehydes,aminos, and ketones. 1971 529 pp. Volume II Presents thepreparations for all monofunctional compounds published between1971 and 1974, plus findings of earlier years to provide a valuablesupplement to Volume I. 1974 437 pp.

Table of Contents

Partial table of contents: Preparation of Acetylenes. Preparation of Carboxylic Acids. Acid Halides and Anhydrides. Preparation of Alcohols and Phenols. Preparation of Aldehydes. Preparation of Alkyls, Methylenes, and Aryls. Preparation of Amides. Preparation of Ethers and Epoxides. Preparation of Halides and Sulfonates. Preparation of Difunctional Compounds.

Volume

v. 12 ISBN 9780471445302

Description

The Compendium of Organic Synthetic Methods series facilitates the working chemist's search for the most useful functional group transformations in organic chemistry. Drawn from an exhaustive survey of the literature, Compendium of Organic Synthetic Methods, Volume 12 contains both functional group transformations and carbon-carbon bond-forming reactions. Author Michael Smith adheres to stringent criteria for listing reactions, including real synthetic utility and reagents that are either readily available or easily prepared and handled in the laboratory. A clear organizational scheme-chemical transformations classified first by reacting functional group of starting material, then by functional group formed-allows for quick reference and information retrieval. Compendium of Organic Synthetic Methods, Volume 12 provides an unparalleled source of information on the methods, reactions, and transformations in contemporary organic chemistry for the working chemist and student alike.

Table of Contents

Preface. Abbreviations. Index, Monofunctional Compounds. Index, Difunctional Compounds. Introduction. 1 Preparation of Alkynes. 2 Preparation of Acid Derivatives. 3 Preparation of Alcohols. 4 Preparations of Aldehydes. 5 Preparation of Alkyls, Methylens, and Aryls. 6 Preparation of Amides. 7 Preparation of Amines. 8 Preparation of Esters. 9 Preparation of Ethyl Epoxides and Thioethers. 10 Preparation of Halides and Sulfonates. 11 Preparation of Hydrides. 12 Preparation of Ketones. 13 Preparation of Nitriles. 14 Preparation of Alkenes. 15 Preparation of Oxides. 16 Preparation of Difunctional Compounds. Author Index.

Volume

v. 8 ISBN 9780471573197

Description

More than a one-volume listing of synthetic methods, Compendium ofOrganic Synthetic Methods offers chemists a highly focused andselective look at several thousand functional grouptransformations. Used by more professionals than any comparablereference on the market, this valuable desktop resource providesquick access to the recipes of the newest, most useful reactionsand transformations. It also affords professionals an unparalleledopportunity to browse the vast body of recent literature for newreactions and transformations that may be of interest. Featuring 1,200 more entries than its predecessor, Volume 8 coversfunctional group transformations and carbon-carbon bond formingreactions appearing in the literature from 1990 through 1992. Itpresents approximately 1,400 examples of published reactions forthe preparation of monofunctional compounds and approximately 1,640examples of reactions that prepare difunctional compounds withvarious functional groups. It also features 60 more reviews thanVolume 7. As in all the previous Compendium volumes, the classificationschemes used allow for quick and easy reference and informationretrieval. Chemical transformations are classified first by thereacting functional group of the starting material and then by thefunctional group formed. The transformation, major reagents thateffect the transformation, yield percentage, and stereochemistryare all clearly shown. The Compendium also includes indices forboth monofunctional and difunctional compounds as an efficientmeans of guiding you to specific classes of transformations. Compendium of Organic Synthetic Methods, Volume 8 providesprofessional chemists and students unparalleled access to thewealth of methods, reactions, and transformations in contemporaryorganic chemistry.

Table of Contents

Preparation of Alkynes. Preparation of Acid Derivatives and Anhydrides. Preparation of Alcohols. Preparation of Aldehydes. Preparation of Alkyls, Methylenes and Aryls. Preparation of Amides. Preparation of Amines. Preparation of Esters. Preparation of Ethers, Epoxides and Thioethers. Preparation of Halides and Sulfonates. Preparation of Hydrides. Preparation of Ketones. Preparation of Nitriles. Preparation of Alkenes. Preparation of Oxides. Preparation of Difunctional Compounds. Author Index.

Volume

v. 7 ISBN 9780471607137

Description

Provides synthetic chemists with a method for rapid retrieval of information from the literature, listing material by reaction type rather than by author name or publication date. Each updated volume presents the latest synthetic methods for preparation of monofunctional and difunctional compounds. The organization is logical and easy to follow; sections are arranged according to the possible interconversions between the major functional groups. Enables synthetic chemists to keep abreast of recent developments and retrieve a specific piece of information quickly and easily.

Table of Contents

Preparation of Alkynes. Preparation of Acid Derivatives and Anhydrides. Preparation of Alcohols. Preparation of Aldehydes. Preparation of Alkyls, Methylenes and Aryls. Preparation of Amides. Preparation of Amines. Preparation of Esters. Preparation of Ethers, Epoxides and Thioethers. Preparation of Halides and Sulfonates. Preparation of Hydrides. Preparation of Ketones. Preparation of Nitriles. Preparation of Alkenes. Preparation of Oxides. Preparation of Difunctional Compounds. Author Index.

Volume

v. 6 ISBN 9780471848967

Description

Provides synthetic chemists with a method for rapid retrieval of information from the literature, listing material by reaction type rather than by author name or publication date. Each updated volume presents the latest synthetic methods for preparation of monofunctional and difunctional compounds. The organization is logical and easy to follow; sections are arranged according to the possible interconversions between the major functional groups. Enables synthetic chemists to keep abreast of recent developments and retrieve a specific piece of information quickly and easily.

Table of Contents

Preparation of Acetylenes. Preparation of Carboxylic Acids, Acid Halides, andAnhydrides. Preparation of Alcohols, Phenols, and Thiols. Preparation of Aldehydes. Preparation of Alkyls, Methylenes, and Aryls. Preparation of Amides. Preparation of Amines. Preparation of Esters. Preparation of Ethers, Epoxides, and Thioethers. Preparation of Halides and Sulfonates. Preparation of Hydrides. Preparation of Ketones. Preparation of Nitriles. Preparation of Oxides. Preparation of Difunctional Compounds. Author Index.

Volume

v. 5 ISBN 9780471867289

Description

Provides synthetic chemists with a method for rapid retrieval of information from the literature, listing material by reaction type rather than by author name or publication date. Each updated volume presents the latest synthetic methods for preparation of monofunctional and difunctional compounds. The organization is logical and easy to follow; sections are arranged according to the possible interconversions between the major functional groups. Enables synthetic chemists to keep abreast of recent developments and retrieve a specific piece of information quickly and easily.

Table of Contents

Abbreviations. Index, Monofunctional Compounds. Index, Difunctional Compounds. Preparation of Acetylenes. Preparation of Carboxylic Acids, Acid Halides, andAnhydrides. Preparation of Alcohols and Phenols. Preparation of Aldehydes. Preparation of Alkyls, Methylenes, and Aryls. Preparation of Amides. Preparation of Amines. Preparation of Esters. Preparation of Ethers and Epoxides. Preparation of Halides and Sulfonates. Preparation of Hydrides. Preparation of Ketones. Preparation of Nitriles. Preparation of Olefins. Preparation of Difunctional Compounds.

Volume

v. 13 ISBN 9781118791684

Description

The Compendium of Organic Synthetic Methods serves as a handy desktop reference for organic chemists to browse new reactions and transformations of interest, facilitating the search for functional group transformations in the original literature of organic chemistry. Volume 13 contains both functional group transformations and carbon-carbon bond forming reactions from the literature in the years 2005-8. It presents examples of published reactions for the preparation of monofunctional compounds. The Compendium of Organic Synthetic Methods series facilitates the search for quality, selected functional group transformations, organized by reacting functional group of starting material and functional group formed, with full references to each reaction Presents examples of published reactions for the preparation of monofunctional compounds from the literature of 2005-8 Provides a handy reference and a valuable tool to the working organic chemist, allowing a quick check of known organic transformations Stringent criteria for inclusion of reactions, including real synthetic utility of reactions, reagents readily available or easily prepared and handled in the laboratory

Table of Contents

Preface vii Introduction ix Index, Monofunctional Compounds xvii Index, Difunctional Compounds xix Abbreviations xxi About the Author xxv 1 Preparation of Alkynes 1 2 Preparation of Acid Derivatives 13 3 Preparation of Acohols 21 4 Preparation of Aldehydes 75 5 Preparation of Alkyls, Methylenes, and Arkyls 89 6 Preparation of Amides 225 7 Preparation of Amines 259 8 Preparation of Esters 303 9 Preparation of Ethers, Epoxides, and Thioethers 325 10 Preparation of Halides and Sulfonates 351 11 Preparation of Hydrides 365 12 Preparation of Ketones 371 13 Preparation of Nitriles 399 14 Preparation of Alkenes 409 15 Preparation of Oxides 433 16 Preparation of Difunctional Compounds 445 Author Index 629

by "Nielsen BookData"

Details

• NCID: BA02839914
• ISBN:
  • 047135550X
  • 0471355518
  • 0471367524
  • 0471049239
  • 0471867284
  • 0471848964
  • 0471607134
  • 0471573191
  • 0471145793
  • 0471202010
  • 0471259659
  • 9780471445302
  • 9781118791684
• LCCN: 71162800
• Country Code: us
• Title Language Code: eng
• Text Language Code: eng
• Place of Publication: New York
• Pages/Volumes: v.
• Size: 24-26 cm
• Classification:
  • NDC8 : 437.01
• Subject Headings:
  • LCSH : Organic compounds -- synthesis
• Parent Bibliography ID:
  • BA00493885