[13]C NMR spectroscopy : a working manual with exercises

著者

    • Breitmaier, E.
    • Bauer, Gerhard

書誌事項

[13]C NMR spectroscopy : a working manual with exercises

Eberhard Breitmaier and Gerhard Bauer ; translated from the German by Bruce K. Cassels

(MMI Press polymer monograph series, v. 3)

Harwood Academic Publishers, c1984

タイトル別名

[13]C-NMR-Spektroskopie

統一タイトル

[13]C-NMR-Spektroskopie

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注記

Translation of: [13]C-NMR-Spektroskopie

Bibliography: p. 345

Includes index

内容説明・目次

内容説明

This demonstrates methods for solving chemical structure problems through the use of 13 C NMR spectra. It aims to guide readers through the functional laboratory methods and applications of 13-carbon resonance in the structure determination of a number of organic compound classes.

目次

  • Basic principles and quantities of nuclear magnetic resonance spectroscopy
  • measurement of 13C-NMR spectra
  • proton decoupling in 13C-NMR spectroscopy
  • chemical methods of signal assignment
  • sample concentration - solvents and standards
  • 13C chemical shifts - a survey
  • interpretation of 13C chemical shifts
  • analysis of coupling constants
  • 13C spin-lattice relaxation times - measurement and range of application
  • exercises in the interpretation of 13C-NMR spectra and their application to structural problems in organic chemistry
  • solutions to the problems in the interpretation of 13C-NMR spectra.

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