書誌事項

Analyses of hazardous substances in air

edited by A. Kettrup ; Working Group Analytical Chemistry, Commission for the Investigation of Health Hazards of Chemical Compounds in the Work Area ; [translator, K.H. Ohrbach]

VCH, c1991-

  • v. 1 : Weinheim
  • v. 1 : New York
  • v. 1 : Weinheim
  • v. 2 : New York
  • v. 3 : Weinheim
  • v. 4 : Weinheim
  • v. 5
  • v. 6
  • v. 7
  • v. 8

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注記

At head of title: DFG, Deutsche Forschungsgemeinschaft

Includes bibliographical references and index

publisher change: WILEY-VCH (vol.4)

内容説明・目次

巻冊次

v. 1 : Weinheim ISBN 9783527270156

内容説明

The determination of hazardous compounds in the air of work areas is an often used procedure for estimating individual exposure to a hazardous substance. This volume comprises 16 analytical methods for determining organic compounds and heavy metals by high pressure liquid chromatography, gas chromatography, infrared spectroscopy and atomic absorption spectrometry. The analytical reliability and reproducibility of these methods have been tested and confirmed; the methods are appropriate for monitoring the adherence to relevant limit values; moreover, they are described in such detail that the technical assistant can use them without having to refer to additional sources; three fundamental chapters on active and diffuse sampling, on quality criteria of analytical methods and on adsorbents are also included.

目次

  • Part 1 Preliminary remarks: introduction
  • theoretical principles of the diffusive sampling - diffusive sampler, basic principles of the diffusion, influence on the diffusive sampling by ambient parameters. Part 2 Valuation of analysis methods and analysis results: definitions
  • functional quality indexes - accuracy of an analysis method, sensitivity of an analysis method, selectivity and specificity of method
  • statistical quality index - accuracy of the method, supply of the statistical data, the uncertainty of the statistical deviation at a few number of measured values, repeatability and reproducibility of analysis results (ISO 5725), detection limit and determination limits of analysis methods, confidence interval for mean values, propagation for standard
  • securing of differences - examination of analysis results, examination of standard deviations. Part 3 Analytical methods: infrared spectrophotometric determination of gases and vapours using long-path glass cuvettes
  • polycyclic aromatic hydrocarbons (PAH)
  • methanol
  • hexamethylene diisocyanate (HDI),2,4- and 2,6-tolylene diisocyanate (TDI 2,4- and 2,6-diisocyanate tolylene)
  • tetraethyl orthosilicate
  • 4,4-methylene-bis(2-chloroaniline)
  • ethylene glycol derivatives
  • 2-methoxyethanol, 2-ethoxyethanol
  • 2-butoxyethanol, 2-methoxyethyl acetate
  • 2-ethoxyethyl acetate
  • furfuryl alcohol
  • carbon disulphide
  • 1-methyl-2-pyrrolidone
  • phenol
  • dimethylethylamine, triethylamine
  • lead
  • nickel
  • cobalt
  • chromium.
巻冊次

v. 1 : Weinheim ISBN 9783527270262

内容説明

This is the second volume in a series of English translations of analytical methods for the determination of occupational toxicants in workplace air. The 16 standardized methods were selected on the basis of the current significance of the compounds dealt with. They meet exceptionally high standards of reliability and reproducibility. Considerable emphasis is placed on sample collection methods and on analytical quality control: every method is checked by at least one examiner. A chapter of adsorbents used for air monitoring purposes provides detailed information on the presently available and used materials.

目次

  • Working Group Analytical Chemistry of the Commission of the Deutsche Forschungsgemeinschaft for the Investigation of Health Hazards of Chemical Compounds in the Work Area
  • Preliminary Remarks
  • Adsorbents for the Adsorption of Organic Compounds
  • 1 General characterization of adsorbents
  • 2 Various adsorbents and their properties
  • 2.1 Inorganic adsorbents
  • 2.1.1 Activated aluminum oxide
  • 2.1.2 Silica gel
  • 2.1.3 Molecular sieves (zeolithes)
  • 2.2 Adsorbents on the basis of carbon
  • 2.2.1 Activated carbon
  • 2.2.2 Graphitized carbon (Carbosieve, Carbopack)
  • 2.3 Porous polymers
  • 2.3.1 Tenax GC
  • 2.3.2 Porapack types
  • 2.3.3 Amberlite XAD synthetic resins
  • 2.3.4 Chromosorb types
  • 3 Summary
  • 4 References
  • Analytical Methods
  • Aldehydes
  • Ammonia
  • Benzotrichloride
  • 2-Bromo-2-chloro-1,1,1-trifluoroethane (Halothane)
  • 2-Butenal
  • 2-Butoxyethylacetate
  • Chlorinated biphenyles (PCB)
  • 1-Chloro-2,3-epoxypropane
  • Dinitrogen oxide
  • Formaldehyde
  • Methanol
  • Pentachlorophenol
  • 2-Propanol
  • 2-Propenal
  • Quartz
  • Total tin
  • Members and Guests of the Working Subgroup.
巻冊次

v. 3 : Weinheim ISBN 9783527270330

内容説明

The analysis of the levels of hazardous substances in the air inhaled by workers in the chemical industry and similar working environments is vital in monitoring adherence to statutory concentration limits and protecting the workers from the adverse effects of such substances. This volume contains 15 standardized methods for the determination of chemical compounds in the air of the work area. All methods are suitable for routine use. They meet exceptionally high standards of reliability and reproducibility. Considerable emphasis is placed on sample collection methods and on analytical quality control. A chapter 'Procedures for the preparation of calibration gas mixtures' provides general information on air monitoring methodology.

目次

Acrylnitrile. 2-Chloroethanol. Ethylene Oxide. Halogenated Narcosis Gases. Methylacrylate. Organotin. Ozone. Phenol. Polyisocyanates. Solvents. Styrene. Tetrahydrofurane. Tetrahydrothiophane. 1,1,1-Trichloroethane. Urea Herbicides.
巻冊次

v. 4 : Weinheim ISBN 9783527270453

内容説明

This text looks at the analysis of levels of hazardous substances in the air inhaled by workers in the chemical industry and similar working environments. It looks at ways of monitoring adherence to statutory concentration limits and protecting workers from the adverse effects of such substances.

目次

  • N-Nitrosamine
  • propyleneoxide
  • 4,4'-diaminodiphenylmethane
  • 2,4-tolylendiamine
  • p-chloroaniline
  • ethyleneoxide
  • vinylchloride.
巻冊次

v. 5 ISBN 9783527270460

内容説明

This is the fifth volume in an international series of analytical methods for the determination of toxicants in the air at the workplace. All methods are reliable, reproducable and meet the requirements for quality control. The analysis of the levels of hazardous substances in the air inhaled by workers in the chemical industry and similar working environments is necessary to monitor adherence to statutory concentration limits and to protect the workers from the adverse effects of such substances.

目次

Analytical Methods.Aldehydes, Method No. 2. Benzene. Bis(chloromethyl)ether (BGI 505 6E). alpha Chlorotoluene (BGI 505 95E). 1,5 Diaminonaphthalene (BGI 505 63E). alpha,alpha Dichlorotoluene (BGI 505 42E). Diethyl sulfate (BGI 505 18E). Dimethyl sulfate (BGI 505 7E). Dinitrotoluenes (BGI 505 60E). Metal working Fluid Aerosols and Vapours. N Nitrosomethylphenylamine and N Nitrosoethylphenylamine (BGI 505 62E). 1,2 Phenylenediamine and 1,3 phenylenediamine (BGI 505 64E). Phosphine. 2,3,7,8 substituted Polychlorinated dibenzodioxins and dibenzofurans (BGI 505 47E). Styrene, Method No. 2. Styrene, Method No. 3. alpha,alpha,alpha Trichlorotoluene (BGI 505 61E). Members and Guests of the Working Subgroup.Contents of the Volumes 1 5.
巻冊次

v. 6 ISBN 9783527270538

内容説明

This is the sixth volume in an international series of analytical methods for the determination of toxicants in the air at the workplace. All methods are reliable, reproducable and meet the requirements for quality control. The analysis of the levels of hazardous substances in the air inhaled by workers in the chemical industry and similar working environments is necessary to monitor adherence to statutory concentration limits and to protect the workers from the adverse effects of such substances.

目次

Preliminary Remarks.Passive Sampling.Quality Control.Analytical Methods.Azinphos methyl. Fenthion. Inorganic Acid Mists (H2SO4, H3PO4). Methabenzthiazuron. Parathion. Polyisocyanates. Solvent Mixtures, Introduction.Solvent Mixtures, Method No. 1.Solvent Mixtures, Method No. 2.Solvent Mixtures, Method No. 3.Solvent Mixtures, Method No. 4.Solvent Mixtures, Method No. 5.Solvent Mixtures, Method No. 6. Volatile Inorganic Acids (HCI, HBr, HNO3).Members and Guests of the Working Subgroup.Contents of the Volumes 1 6.
巻冊次

v. 7 ISBN 9783527277926

内容説明

This is the seventh volume in an international series of analytical methods for the determination of toxicants in the air at the workplace. All methods are reliable, reproducable and meet the requirements for quality control. The analysis of the levels of hazardous substances in the air inhaled by workers in the chemical industry and similar working environments is necessary to monitor adherence to statutory concentration limits and to protect the workers from the adverse effects of such substances.

目次

Analytical Methods.Acrylamide (BGI 505-37E).Antimony trioxide (BGI 505-29E).1,3-Butadiene (BGI 505-26E).cis-1,3-dichloropropene and trans-1,3-dichloropropene (BGI 505-55E).Dimethylcarbamoyl chloride (BGI 505-35E).Dimethylsulfamoyl chloride (BGI 505-43E).2,6-Dinitrotoluene (BGI 505-40E).1,2-Epoxybutane (BGI 505-56E).4,4'-Methylene-bis(2-chloroaniline) (BGI 505-38E).2-Naphthylamine (BGI 505-9E).Nickel (BGI 505-10E).2-Nitronaphthalene (BGI 505-22E).o-Toluidine (BGI 505-49E).Members of the Analytical Group of the Expert Committee "Chemistry.Contents of Volumes 1-7.
巻冊次

v. 8 ISBN 9783527277933

内容説明

This eighth volume in the series provides standardized methods for analyzing chemical compounds of current significance in industrial medicine. All the methods are reliable, reproducible and meet the requirements for quality control. In each case, a description is given of the general principles involved, details of equipment, chemicals and solution preparation, calibration standards, sample collection and preparation, experimental conditions, procedure for calibration and analysis, calculation of results, performance evaluation, discussion and references. Throughout, considerable emphasis is placed on sample collection methods and on analytical quality control: every method is checked by at least one examine.

目次

Working Group "Analytical Chemistry" of the Commission of the Deutsche Forschungsgemeinschaft for the Investigation of Health Hazards of Chemical Compounds in the Work Area.Analytical Methods.Acetamide.Alkali metal hydroxides and alkaline earth hydroxides.Alkanolamines.Atrazin Method No. 1.Benzotriazoles.Chlorinated biphenyls (PCBs).Furfuryl alcohol.Gelatinous explosives.Hydrogen peroxide.Lacquer aerosols Method No. 1.Lacquer aerosols Method No. 2.Lacquer aerosols Method No. 3.Pentachlorophenol and Lindane.PAHs Method No. 2.PAHs Method No. 3.Sulfur dioxide.Members and Guests of the Working Subgroup.Contents of Volumes 1-8.

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詳細情報

  • NII書誌ID(NCID)
    BA13793553
  • ISBN
    • 3527270159
    • 0895739011
    • 3527270264
    • 1560812753
    • 3527270337
    • 3527270450
    • 3527270469
    • 3527270531
    • 3527277927
    • 3527277935
  • 出版国コード
    gw
  • タイトル言語コード
    eng
  • 本文言語コード
    eng
  • 原本言語コード
    ger
  • 出版地
    Weinheim (Federal Republic of Germany) ; New York
  • ページ数/冊数
    v.
  • 大きさ
    25 cm
  • 件名
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