High resolution XPS of organic polymers : the Scienta ESCA300 database
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書誌事項
High resolution XPS of organic polymers : the Scienta ESCA300 database
Wiley, 1992
- タイトル別名
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Scienta ESCA300 database
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注記
Includes bibliographical references and index
内容説明・目次
内容説明
This database examines the use of the Scienta ESCA300 spectrometer in polymer surface analysis. The prototype, developed jointly with ICI, has been used in the systematic reinvestigation of over 100 standard homo polymers. It provides the full spectral information: survey and core line regions (with fitted components), shake-up spectra, valence bands and in some cases, Auger spectra. All the data are parameterized and tabulated, and full details of sample preparation etc. are given. The instrument performance and operating conditions are extensively documented.
目次
- Description of the spectrometer
- x-ray source
- monochromator
- electron lens
- hemispherical analyser
- multichannel detector
- sample analysis chamber
- charge compensation
- performance on conducting samples
- performance on insulating samples
- performance on testing of the spectrometer
- experimental protocol
- sample mounting
- data acquisition
- correction of binding energy scale for sample charging
- curve fitting
- lineshapes
- shake-up structure
- valence bands
- impurities
- x-ray degradation
- organization of the database
- list of polymers and acronyms
- the database
- appendix 1 - primary C 1s shifts
- appendix 2 - secondary C 1s shifts
- appendix 3.1 - 0 1s binding energies in CHO polymers
- appendix 3.2 - 0 1s binding energies in other polymers
- appendix 4 - N 1s binding energies
- appendix 5 - F 1s binding energies
- appendix 6 - binding energies and spin-orbit constants for core-line doublets
- apendix 7 - binding energies of peaks appearing in the valence band region.
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