CiNii 図書 - High resolution XPS of organic polymers : the Scienta ESCA300 database

This database examines the use of the Scienta ESCA300 spectrometer in polymer surface analysis. The prototype, developed jointly with ICI, has been used in the systematic reinvestigation of over 100 standard homo polymers. It provides the full spectral information: survey and core line regions (with fitted components), shake-up spectra, valence bands and in some cases, Auger spectra. All the data are parameterized and tabulated, and full details of sample preparation etc. are given. The instrument performance and operating conditions are extensively documented.

Description of the spectrometer
x-ray source
monochromator
electron lens
hemispherical analyser
multichannel detector
sample analysis chamber
charge compensation
performance on conducting samples
performance on insulating samples
performance on testing of the spectrometer
experimental protocol
sample mounting
data acquisition
correction of binding energy scale for sample charging
curve fitting
lineshapes
shake-up structure
valence bands
impurities
x-ray degradation
organization of the database
list of polymers and acronyms
the database
appendix 1 - primary C 1s shifts
appendix 2 - secondary C 1s shifts
appendix 3.1 - 0 1s binding energies in CHO polymers
appendix 3.2 - 0 1s binding energies in other polymers
appendix 4 - N 1s binding energies
appendix 5 - F 1s binding energies
appendix 6 - binding energies and spin-orbit constants for core-line doublets
apendix 7 - binding energies of peaks appearing in the valence band region.

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High resolution XPS of organic polymers : the Scienta ESCA300 database

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