Chromatography of mycotoxins : techniques and applications

Bibliographic Information

Chromatography of mycotoxins : techniques and applications

edited by Vladimír Betina

(Journal of chromatography library, v. 54)

Elsevier, 1993

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Note

Includes bibliographical references and index

Description and Table of Contents

Description

This work comprises two parts: Part A - Techniques, and Part B - Applications. In Part A the most important principles of sample preparation, extraction, clean-up, and of established and prospective chromatographic techniques are discussed in relation to mycotoxins. In Part B the most important data, scattered in the literature, on thin-layer, liquid, and gas chromatography of mycotoxins have been compiled. Mycotoxins are mostly arranged according to families, such as aflatoxins, trichothecenes, lactones, and so on. Chromatography of individual important mycotoxins and multi-mycotoxin chromatographic analyses are also included. Applications are presented in three chapters devoted to thin-layer, liquid, and gas chromatography of mycotoxins.

Table of Contents

  • Part A Techniques: 1. Sampling, Sample Preparation, Extraction and Clean-up, V. Betina: Sampling and Sample Preparation
  • Sample Extraction and Clean-up
  • Illustrative Example. 2. Techniques of Thin Layer Chromatography, R.D. Coker et al: Clean-up Methods
  • Normal Phase TLC
  • Reverse-phase TLC (RPTLC)
  • High Performance Thin Layer Chromatography (HPTLC)
  • Preparative TLC
  • Detection
  • Quantitative and Semi-Quantitative Evaluation
  • Illustrative example. 3. Techniques of Liquid Column Chromatography, P. Kuronen: Sample Pretreatment
  • Column Chromatography
  • Mini-Column Chromatography
  • High-Performance Liquid Chromatography. 4. Techniques of Gas Chromatography, R.W. Beaver: Resolution in Gas Chromatography
  • Extracolumn Resolution. 5. Emerging Techniques: Immunoaffinity Chromatography, A.A.G. Candlish and W. H. Stimson
  • Immunoaffinity Chromatography Theory
  • Practical Aspects and Instrumentation
  • Sample Preparation
  • Illustrative Examples. 6. Emerging Techniques - Enzyme-Linked lmmunosorbent Assay (ELISA) as Alternatives to Chromatographic Methods: C. M. Ward et al: Principles of ELISA
  • Sample Preparation
  • Instrumentation and Practice
  • Illustrative Examples. Part B Applications: 7. Thin-Layer Chromatography of Mycotoxins, V. Betina: Aflatoxins
  • Sterigmatocystin and Related Compounds
  • Trichothecenes
  • Small Lactones
  • Macrocyclic Lactones
  • Ochratoxins
  • Rubratoxins
  • Hydroxyanthraquinones
  • Epipolythiopiperazine-3,6-diones
  • Tremorgenic Mycotoxins
  • Alternaria Toxins
  • Citrinin
  • G-Cyclopiazonic Acid
  • PR Toxin and Roquefortine
  • Xanthomegnin, Viomellein and Vioxanthin
  • Naphtho-y-Pyrones
  • Secalonic Acids
  • TLC of Miscellaneous Toxins
  • Multi-Mycotoxin TLC
  • TLC in Chemotaxonomic Studies of Toxigenic Fungi. 8. Liquid Column Chromatography of Mycotoxins, J.C. Frisvad and U. Thrane: Column Chromatography
  • Mini-Column Chromatography
  • High Performance Liquid Chromatography
  • Informative On-line Detection Methods. 9. Gas Chromatography of Mycotoxins, P.M. Scott: Trichothecenes
  • Zearalenone
  • Moniliformin
  • Alternaria Toxins
  • Slaframine and Swainsonine
  • Patulin
  • Penicillic Acid
  • Sterigmatocystin
  • Aflatoxins
  • Ergot Alkaloids
  • Miscellaneous Mycotoxins.

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