Preparation of alkenes : a practical approach
著者
書誌事項
Preparation of alkenes : a practical approach
(The practical approach in chemistry series)
Oxford University Press, 1996
- : hbk
- : pbk
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注記
Includes bibliographical references and index
内容説明・目次
- 巻冊次
-
: pbk ISBN 9780198557944
内容説明
This book describes the experimental methods needed for the preparation of alkenes using many methods. The techniques and procedures used are an important aspect of laboratory work. The methods employed in this practical approach have been carefully reviewed and practical details and tips are offered. In individual chapters the authors share their experience of chemical reactions to provide background information and invaluable protocols for the synthesis of alkenes.
Particular attention is paid to controlling the geometry of alkene synthesis. Easy to follow step-by-step guides which can be used at the bench as well as references to examples in recent literature make this an ideal accompaniment for practising synthetic chemists in academic and industrial
research.
目次
- 1. Introducton and general methods
- 2. The Wittig reaction and related methods
- 3. Non-phosphorus stabilised carbanions in alkene synthesis
- 4. Chromium - and titanium-mediated synthesis of alkenes from carbonyl compounds
- 5. Elimination and addition-elimination reactions
- 6. Reduction of alkynes
- 7. Reactiotn of alkynes with organometallic reagents
- 8. Catalytic coupling reactions
- 9. Summary of alkene synthesis
- Appendix 1: Summary of Protocols (affording alkenes)
- Appendix 2: List of suppliers
- Index
- 巻冊次
-
: hbk ISBN 9780198557951
内容説明
This book describes the experimental methods needed for the preparation of alkenes using many methods. The techniques and procedures used are an important aspect of laboratory work. The methods employed in this practical approach have been carefully reviewed and practical details and tips are offered. In individual chapters the authors share their experience of chemical reactions to provide background information and invaluable protocols for the synthesis of alkenes. Particular attention is paid to controlling the geometry of alkene synthesis. Easy to follow step-by-step guides which can be used at the bench as well as references to examples in recent literature make this an ideal accompaniment for practising synthetic chemists in academic and industrial research. This book is intended for practising synthetic organic chemists in academic and industrial research.
目次
1: Introducton and general methods. 2: The Wittig reaction and related methods. 3: Non-phosphorus stabilised carbanions in alkene synthesis. 4: Chromium - and titanium-mediated synthesis of alkenes from carbonyl compounds. 5: Elimination and addition-elimination reactions. 6: Reduction of alkynes. 7: Reactiotn of alkynes with organometallic reagents. 8: Catalytic coupling reactions. 9: Summary of alkene synthesis. Appendix 1: Summary of Protocols (affording alkenes). Appendix 2: List of suppliers. Index
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