Pilot plants and scale-up of chemical processes
著者
書誌事項
Pilot plants and scale-up of chemical processes
（Special publication / Royal Society of Chemistry, v. 195,
Royal Society of Chemistry, c1997-1999
- [I]
- II
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注記
Includes index
内容説明・目次
- 巻冊次
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II ISBN 9780854047192
内容説明
How do you translate bench chemistry into 10 -100 litre pilot plant scale? Drawing on the wealth of experience of its expert contributors, Pilot Plants and Scale-up of Chemical Processes II provides an insight into how methods, procedures and techniques can be optimised. Up-to-date and highly focused, this book addresses topics including the choice of phase-transfer catalyst, safe scale-up of both Grignard and organolithium reactions, and on-line techniques for examining crystallisation. Newly established collaborative industry/academia projects are discussed, along with other procedures that have a practical application in industry. As a source of innovative techniques and best current practice, this book is a must for process development and pilot plant chemists as well as chemical engineers.
目次
- Speciality chemical manufacturing in the UK - has it a future?
- chemical aspects of scale-up
- choosing a phase-transfer catalyst to enhance reactivity and catalyst separation, part 1
- a new on-line batch process engineering facility for examining the crystallisation of organic speciality chemical products
- the safe scale-up of a Grignard Reaction using an in-situ reaction monitoring technique
- process development and scale-up of organolithium reactions
- oft forgotten physical chemical laws or fire, explosion and chemical reaction hazards during scale-up.
- 巻冊次
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[I] ISBN 9780854047963
内容説明
One of the biggest challenges facing today's chemist and chemical engineer is the translation of bench chemistry to the pilot plant. This book provides expert insights into current best practice, and will prove an indispensable manual for all those involved in pilot plant design and scale-up implementation - process chemists, engineers and managers alike. The international expertise of the contributors covers a wide range of topics, and new material covered includes: the removal of heavy metals from effluent, heat flow calorimetry, low temperature processes, good manufacturing practice in pilot plants, design issues, the use of statistical methods in the running of pilot plants. Pilot Plants and Scale-Up of Chemical Processes is a must for all those who are, and wish to remain, expert in the field, providing for the first time in print, a comprehensive and unique perspective of pilot plant production.
目次
- Design and Control
- The Role of Chemical Engineers in the Design and Operation of Pilot Plants
- Batch Versus Continuous Processing
- Control and Automation of Batch Processes
- General Techniques
- Good Manufacturing Practice Applied to Pilot Plants
- The Application of Statistical Methods to Pilot Plants
- Experiences in Heat Flow Calorimetry and Thermal Analysis
- Specific Techniques
- Heavy Metal from Effluent - Process Development from Laboratory through Pilot Plant
- Plant Scale Reactions Down to -100|C
- Subject Index.
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