Principles and practice
著者
書誌事項
Principles and practice
（Handbook of thermal analysis and calorimetry / series editor, Patrick K. Gallagher, v.1）
Elsevier, 1998
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注記
Includes bibliographical references and index
内容説明・目次
内容説明
Handbook of Thermal Analysis and Calorimetry, Volume 1: Principles and Practice describes the basic background information common to thermal analysis and calorimetry in general. Thermodynamic and kinetic principles are discussed along with the instrumentation and methodology associated with thermoanalytical and calorimetric techniques. The purpose is to collect the discussion of these general principles and minimize redundancies in the subsequent volumes that are concerned with the applications of these principles and methods. More unique methods, which pertain to specific processes or materials, are covered in later volumes.
目次
- Definitions, nomenclature, terms and literature: thermal analysis and calorimetry - definitions, classifications and nomenclature
- characterization of measuring instruments
- characterization of measuring instruments
- characterization of measured curves and values
- characterization, interpretation and representation of results
- literature in thermal analysis and calorimetry. Part 2 Thermodynamic background to thermal analysis and calorimetry: thermodynamic systems and the concept of temperature
- the first law of thermodynamics
- the second and third laws of thermodynamics
- the Helmholtz energy and the Gibbs energy
- equilibrium conditions
- open systems
- systems consisting of a pure substance
- mixtures and phase diagrams
- chemical reactions. Part 3 Kinetic background to thermal analysis and calorimetry: kinetic models for solid-state reactions
- the most important rate equations used in kinetic analyses of solid state reactions
- kinetic analysis of isothermal experiments
- the influence of temperature on reaction rate
- kinetic analysis of non-isothermal experiments
- kinetic apsects of non-scanning calorimetry
- publication of kinetic results. Part 4 Thermogravimetry and thermomagnetometry: measurement of mass
- design and control of the thermobalance
- data collection and presentation
- calibration. Part 5 Differential thermal analysis and differential scanning calorimetry: introduction and historical background
- definitions and distinctions
- theory of DTA and DSC
- instrumentation
- modulated temperature differential scanning calorimetry (MTDSC)
- operations and sampling
- general interpretation and conclusion. Part 6 Thermomechanical methods: static methods
- dynamic mechanical thermal analysis (DMTA). Part 7 Dielectric techniques: dielectric response
- temperature dependence
- effect of moisture content
- instrumentation
- nomenclature. Part 8 Controlled rate thermal analysis and related techniques: historical development
- different properties and modes used for SCTA
- nomenclature
- the advantages of SCTA
- kinetic aspects
- prospects for the future. Part 9 Less-common techniques: emanation thermal analysis (ETA)
- thermosonimetry
- thermoacoustimetry. Part 10 Thermomicroscopy: general equipment and accessories
- experimental methods
- examples of applications. (Part contents)
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