Split and splitless injection for quantitative gas chromatography : concepts, processes, practical guidelines, sources of error
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Bibliographic Information
Split and splitless injection for quantitative gas chromatography : concepts, processes, practical guidelines, sources of error
Wiley-VCH, c2001
4th, completely revised ed.
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Note
Includes index
Description and Table of Contents
Description
This comprehensive and unique handbook of split and splitless injection techniques has been completely revised and updated. This new edition offers: new insights concerning sample evaporation in the injector; information about matrix effects; and a new chapter on injector design. The real processes within the injector are for the first time visualized and explained by the CD-ROM included in the book. Furthermore the reader will understand the concepts of injection techniques and get a knowledge of the sources of error. The handbook also includes many practical guidelines. From reviews of former editions: "This substantial book is on injection techniques alone, which...demonstrates this can have many pitfalls...no one should be allowed to direct a laboratory doing quantitative analysis by GC without first being thoroughly familar with this book..." - "The Analyst". "This is a detailed reference volume filled with practical suggestions and techniques for managing split and splitless injection in the day-to-day world of the working gas chromatographer. It will be useful...for anyone who must work hands-on with GC." - "Journal of High Resolution Chromatography".
Table of Contents
PART A: SYRINGE NEEDLE. Syringe Needle Handling Techniques. Evaporation Inside Needle. Possibilities of Avoiding Evaporation in the Needle. Sample Volume. Solvents and Solutes. PART B: SAMPLE EVAPORATION IN THE INJECTOR. Vaporizing Chamber. Evaporation Time. Amount of Heat Required. Sources of Heat. Problems Caused by Incomplete Evaporation. PART C: SPLIT INJECTION. The Split Ratio. Sample Concentration Suitable for Split Injection. Split Injection for Fast Analysis. Analysis Requiring Maximum Sensitivity. High Split Ratios for Reducing Sample Size. Problems Concerning the Split Ratio. Problems Concerning the Linearity of Splitting. PART D: SPLITLESS INJECTION. How to Perform Splitless Injection. Sample Volumes Suitable for Splitless Injection. Splitless Injection of Large Volumes. General Evaluation of Splitless Injection. PART E: INJECTOR DESIGN. Design for Split Injection Design for Splitless Injection.
by "Nielsen BookData"
