Organic chemistry laboratory : with qualitative analysis : standard and microscale experiments
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書誌事項
Organic chemistry laboratory : with qualitative analysis : standard and microscale experiments
Brooks/Cole Thomson Learning, c2001
3rd ed.
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注記
Includes index
内容説明・目次
内容説明
The new edition continues to offer a wide variety of organic lab experiments for both standard and microscale formats and features unusually strong coverage of spectroscopy.
目次
1. Introduction. 2. Melting Points. 3. Recrystallization. 4. Extraction. 5. Distillation. 6. Gas Chromatography. 7. Column Chromatography. 8. Thin Layer Chromatography. 9. High Performance Liquid Chromatography. 10. Steam Distillation of Essential Oils. 11. Infrared Absorption Spectroscopy. 12. Spectroscopic Structure Determination: A Lifelong Quest. 13. Proton Nuclear Magnetic Resonance. 14. Advanced Structure Determination. 15. The Literature of Organic Chemistry. 16. Properties of Hydrocarbons. 17. Nucleophylic Substitution of Alkyl Halides. 18. Properties of Alcohols. 19. The Grignard Reaction. 20. Dehydration of Alcohols. 21. Oxidation and Reduction. 22. Aldehydes and Ketones. 23. Determination of pK(a): Effects of Substituents on Acidity. 24.Carboxylic Acid Mini-unknown. 25. Esterification and Saponification: Effect of Substituents on Reactivity. 26. Friedel-Crafts Alkylation and Acylation. 27. Aromatic Nitration. 28. Aromatic Nucleophilic Substitution. 29. Properties of Amines. 30. Chemiluminescence. 31. Photodimerization of Benzophenone. 32. The Diels-Alder Reaction. 33. Phase Transfer Catalysis. 34. Derivatives of Caroboxylic Acids: Synthesis of a Plant Hormone. 35. Synthesis of Coumarin. 36. Benzyne. 37. Heterocyclic Syntheses: Pyrimidines, Pyridones, Isoxazoles, Quinolines, and Indoles. 38. Heterocyclic Synthesis: Phenytoin. 39. Synthesis of Sulfanilamide. 40. Resolution of a-Phenylethylamine. 41. Chemistry of Sugars. 42. Acid-Catalyzed and Enzyme-Catalyzed Hydrolosis of Polysaccharides. 43. Analysis of Fats and Oils. 44. Synthetic Organic Polymers. 45. Dyes and Dyeing. 46. Qualitative Organic Analysis. Appendix A: Selected Atomic Weights. Appendix B: Common Acids and Bases. Appendix C: Common Organic Liquids. Appendix D: Representative Calculations.
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