Basic one- and two-dimensional NMR spectroscopy
著者
書誌事項
Basic one- and two-dimensional NMR spectroscopy
Wiley-VCH, c2005
4th, completely rev. and updated ed
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注記
Includes bibliographical references and indexes
内容説明・目次
内容説明
This classic textbook for all users of NMR spectroscopy shows the basics of this technique and how to interpret the spectra. Covering the material taught in graduate courses, this text provides both students and professionals with a lucid introduction, thoroughly explaining the underlying theory but with a minimum of mathematics. Written by an NMR expert with long-standing teaching experience, this thoroughly enlarged and updated fourth edition includes - polymer solid state NMR; analysis of biopolymers; and, applications of magnetic resonance tomography and magnetic resonance spectroscopy. With its layout and illustrations designed for maximum clarity, this is a must for students and lecturers in chemistry, biochemistry, pharmacy, as well as spectroscopists. From reviews of previous editions: "This book deserves much praise...The book forms an excellent bridge between the very simple texts on spectral interpreataion and more specialist works with an emphasis on mathematical theory...The many diagrams are clear and of high quality, and the examples of NMR spectra throughout the book are well chosen.
This book is highly educational and will be of benefit to those who have to teach NMr and to students and scientists in academic and industrial laboratories who use NMR spectroscopy." - "NMR in Biomedicine". "This is an excellent book...we have been using the first edition of the book in our graduate course in NMR for three years and have been very pleased with it. My opinion is that someone who began knowing nothing about NMR could become quite proficient at structure determination by simply mastering the contents of this book. I highly recommend it." - "Journal of the American Chemical Society". "Almost every course in chemistry and biochemistry nowadays has some NMR component, and the student's interest depends on how the material is delivered. This book is a pleasure to read and if it does not arouse the student's interest, then it is difficult to see what could. It is clearly written and illustrated, with a near perfect balance of mathematics and text." - "Chemistry in Britain".
目次
1 The Physical Basis of NMR Spectroscopy. 1.1 Introduction. 1.2 Nuclear Angular Momentum and Magnetic Moment. 1.3 Nuclei in a Static Magnetic Field. 1.4 Basic Principles of the NMR Experiment. 1.5 The Pulsed NMR Method. 1.6 Spectral Parameters: a Brief Survey. 1.7 "Other" Nuclides. 1.8 Bibliography for Chapter 1. 2 The Chemical Shift. 2.1 Introduction. 2.2 1H Chemical Shifts of Organic Compounds. 2.3 13C Chemical Shifts of Organic Compounds. 2.4 Relationships between the Spectrum and the Molecular Structure. 2.5 Chemical Shifts of "Other" Nuclides. 2.6 Bibliography for Chapter 2. 3 IndirectSpin-Spin Coupling. 3.1 Introduction. 3.2 H,H Coupling Constants and Chemical Structure. 3.3 C,H Coupling Constants and Chemical Structure. 3.4 C,C Coupling Constants and Chemical Structure. 3.5 Correlations between C,H and H,H Coupling Constants. 3.6 Coupling Mechanisms. 3.7 Couplings of "Other" Nuclides (Heteronuclear Couplings). 3.8 Bibliography for Chapter 3. 4 Spectrum Analysis and Calculations. 4.1 Introduction. 4.2 Nomenclature. 4.3 Two-Spin Systems. 4.4 Three-Spin Systems. 4.5 Four-Spin Systems. 4.6 Spectrum Simulation and Iteration. 4.7 Analysis of 13C NMR Spectra. 4.8 Bibliography for Chapter 4. 5 Double Resonance Experiments. 5.1 Introduction. 5.2 Spin Decoupling in 1HNMR Spectroscopy. 5.3 Spin Decoupling in 13C NMR Spectroscopy. 5.4 Bibliography for Chapter 5. 6 Assignment of 1H and 13C Signals. 6.1 Introduction. 6.2 1HNMR Spectroscopy. 6.3 13C NMR Spectroscopy. 6.4 Computer-aided Assignment of 13C NMR Spectra. 6.5 Bibliography for Chapter 6. 7 Relaxation. 7.1 Introduction. 7.2 Spin-Lattice Relaxation of 13C Nuclei (T1). 7.3 Spin-Spin Relaxation (T2). 7.4 Bibliography for Chapter 7. 8 One-Dimensional NMR Experiments using Complex Pulse Sequences. 8.1 Introduction. 8.2 Basic Techniques Using Pulse Sequences and Pulsed Field Gradients. 8.3 The J-Modulated Spin-Echo Experiment. 8.4 The Pulsed Gradient Spin-Echo Experiment. 8.5 Signal Enhancement by Polarization Transfer. 8.6 The DEPT Experiment. 8.7 The Selective TOCSY Experiment. 8.8 The One-Dimensional INADEQUATE Experiment. 8.9 Bibliography for Chapter 8. 9 Two-Dimensional NMR Spectroscopy. 9.1 Introduction. 9.2 The Two-Dimensional NMR Experiment. 9.3 Two-Dimensional J-Resolved NMR Spectroscopy. 9.4 Two-Dimensional Correlated NMR Spectroscopy. 9.5 The Two-Dimensional INADEQUATE Experiment. 9.6 Summary of Chapters 8 and 9. 9.7 Bibliography for Chapter 9. 10 The Nuclear Overhauser Effect. 10.1 Introduction. 10.2 Theoretical Background. 10.3 Experimental Aspects. 10.4 Applications. 10.5 Bibliography for Chapter 10. 11 Dynamic NMR Spectroscopy (DNMR). 11.1 Introduction. 11.2 Quantitative Calculations. 11.3 Applications. 11.4 Bibliography for Chapter 11. 12 Shift Reagents. 12.1 Lanthanide Shift Reagents (LSRs). 12.2 Chiral Lanthanide Shift Reagents. 12.3 Chiral Solvents. 12.4 Bibliography for Chapter 12. 13 Macromolecules. 13.1 Introduction. 13.2 Synthetic Polymers. 13.3 Biopolymers. 13.4 Bibliography for Chapter 13. 14 NMR Spectroscopy in Biochemistry and Medicine. 14.1 Introduction. 14.2 Elucidating Reaction Pathways in Biochemistry. 14.3 High-Resolution in vivo NMR Spectroscopy. 14.4 Magnetic Resonance Tomography. 14.5 Bibliography for Chapter 14. Subject Index. Index of Compounds.
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