More practical problem solving in HPLC
著者
書誌事項
More practical problem solving in HPLC
Wiley-VCH, c2005
- : pbk
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注記
Includes index
内容説明・目次
内容説明
A unique approach to solving HPLC problems. Everyone who bought "Problem Solving in HPLC" by Stavros Kromidas will equally benefit from nearly 100 new practical examples for optimization, trouble-shooting, and instrument performance given in this sequel. The author provides guidance for selecting and evaluating methods, intstruments and columns practical help with everyday trouble-shooting advice for optimizing separations, always explaining the reason why. In each case the problem, the solution and the conclusions are presented over a maximum of 4 pages, and in addition the book contains manufacturers' addresses, references, data tables and checklists.
目次
Preface. The Structure of the Book. In Lieu of an Introduction. Crosswords. Across. Down. An HPLC-Quiz. An HPLC Tale. 1. HPLC TIPS. 1.1 Stationary Phases, Columns (Tips 1-11). 1.2 Buffers, pH Value (Tips 12-21). 1.3 Optimization, Peak Homogeneity (Tips 22-37). 1.4 Troubleshooting (Tips 38-55). Have A Break... Dear Reader. Complete the Sentences. "Matching Pairs". Has Peaky Remembered His Lesson Correctly? 1.5 General HPLC Tips (Tips 56-73). Literature HPLC Tips. 2. LC-MS COUPLING, MICRO- and NANO-LC, QUANTIFICATION. 2.1 LC-MS Coupling (Tips 74-81). 2.2 Micro and Nano LC (Tips 82-91). 2.3 Quantification. 3. Appendix. 3.1 Solutions to Quantification Problems. 3.2 From Theory to Practice-Empirical Formulae, Rules of Thumb and Simple Relationships in Everyday HPLC. 3.3 Information Resources for Analysis/HPLC. 3.4 Analytical Chemistry Today. 3.5 Trends in HPLC. 3.6 Thoughts about a Dead Horse. Index.
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